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        <title>Frontiers in Materials | Structural Materials section | New and Recent Articles</title>
        <link>https://www.frontiersin.org/journals/materials/sections/structural-materials</link>
        <description>RSS Feed for Structural Materials section in the Frontiers in Materials journal | New and Recent Articles</description>
        <language>en-us</language>
        <generator>Frontiers Feed Generator,version:1</generator>
        <pubDate>2026-07-29T09:11:49.637+00:00</pubDate>
        <ttl>60</ttl>
        <item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1867691</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1867691</link>
        <title><![CDATA[Data-driven prediction and engineering validation of early-age autogenous shrinkage in UHPC]]></title>
        <pubdate>2026-07-29T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Shijun Wang</author><author>Teng Tong</author><author>Wenming Zhang</author><author>Meng-En Yue</author><author>Xu Wang</author>
        <description><![CDATA[Early-age autogenous shrinkage remains a major obstacle to the durable use of ultra-high-performance concrete (UHPC), because the response is controlled by coupled mixture, curing, age and restraint effects. This study develops a data-driven prediction workflow from an external database containing 7678 UHPC shrinkage records and nine mixture, mechanical and curing descriptors. Mask-related columns were removed, true zero contents for supplementary cementitious materials and steel fibers were retained, and nonphysical zeros were imputed within each training fold. Pearson analysis showed weak single-variable correlations with shrinkage (|r| < 0.20), confirming the need for nonlinear models. BPNN, RF and XGBoost were evaluated using shuffled five-fold cross-validation and a high-shrinkage-sensitive training workflow. Based on the reported prediction-comparison dataset, RF and XGBoost achieved the strongest global agreement, with R2 values of 0.823 and RMSE values close to 112 με, whereas BPNN gave R2 = 0.774, RMSE = 126.62 με and MAE = 63.95 με. The high-shrinkage tail, uniformly defined as measured shrinkage greater than 1,000 με, remained more difficult: for these 226 records, the mean biases were −109.9, −111.6 and −128.6 με for BPNN, RF and XGBoost, respectively. These results indicate that UHPC shrinkage prediction from literature-derived curve points requires both global accuracy reporting and explicit tail-error checking. The model was further linked to bridge-deck monitoring data to distinguish material-level free autogenous shrinkage from restrained field response.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1886423</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1886423</link>
        <title><![CDATA[Study on mechanical response of subgrade soil based on composite micro-expansive piles material]]></title>
        <pubdate>2026-07-24T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Xinyu Yao</author><author>Guangcheng Zhang</author><author>Yu Liu</author><author>Hongliu Rong</author><author>Fujia Meng</author>
        <description><![CDATA[IntroductionTo enhance the inherent shear resistance of in-service highway subgrade soils and effectively improve subgrade safety resilience under short-term traffic closure conditions, this study proposes a technical scheme of installing actively-compacted micro-expansive piles.MethodsUtilizing field-measured parameters of the subgrade soils and micro-expansive piles materials, a finite element model was established to analyze the effects of radial stresses (10 kPa, 50 kPa, 100 kPa) induced by various expansion rates on the stress distribution of the subgrade, as well as the influence of different diameter-to-spacing ratios (0.2, 0.4, 0.6) on the overall shear resistance of the subgrade.ResultsThe results indicate that when the diameter-to-spacing ratio is 0.2, the radial stress attenuates by 89.53%–95.82% at the midpoint between two piles, indicating a limited effective stress transmission distance. Increasing the diameter-to-spacing ratio to 0.6 reduces the attenuation to 24.05%–25.15%, resulting in a more uniform stress distribution. Under a diameter-to-spacing ratio of 0.6 and a radial stress of 100 kPa, the maximum principal stress at the limit equilibrium state of the subgrade soils within the pile-influenced depth (0–5 m) is enhanced by an average of 60.5%.DiscussionThis study demonstrates that appropriately configured radial stress and diameter-to-spacing ratios can significantly enhance the subgrade’s resistance to shear failure, providing a scientifically effective approach for improving the safety resilience of in-service highway subgrades.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1879511</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1879511</link>
        <title><![CDATA[Printability and mix design optimization of microencapsulated phase-change concrete for 3D printing]]></title>
        <pubdate>2026-07-22T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Jingjing He</author><author>Ran Tang</author><author>Zhihao He</author><author>Haiwei Wang</author><author>Xinchao Zheng</author><author>Fang Liu</author><author>Fangping Li</author>
        <description><![CDATA[To mitigate the environmental impact associated with the high cement consumption in conventional 3D printable concrete (3DPC) and to enhance the intelligent thermal regulation capacity of modern buildings in complex environments, a novel 3D printable phase-change concrete incorporating industrial solid wastes was developed in this study. Through comprehensive assessments of fluidity, extrudability, and buildability, the critical workability control parameters satisfying the requirements of continuous 3D printing were determined. Subsequently, the response surface methodology based on a Box-Behnken design was employed to analyze the individual and interactive effects of silica fume content, microencapsulated phase-change materials dosage, and water-to-binder (W/B) ratio on the 28-day compressive strength of the 3D printed specimens. The analysis of variance results indicated that the significance of these three factors on compressive strength followed a descending order of W/B ratio > mPCMs dosage > silica fume content. Furthermore, all factors exhibited a highly significant non-linear quadratic effect, characterized by an initial increase followed by a subsequent decrease. A single-response optimization algorithm was utilized to determine the optimal mixture design, targeting the maximization of mechanical properties under a fixed printability constraint: a W/B ratio of 0.265, a silica fume content of 7.22%, and an mPCMs dosage of 2.72%. Experimental validation demonstrated that the measured 28-day compressive strength of the optimal mixture was 46.54 MPa, yielding a relative error of only 6.26% compared to the predicted value. This confirmed the high accuracy and reliability of the established quadratic regression prediction model. This study provides a reliable material foundation and scientific basis for the development of highly efficient 3D printed concrete components with integrated thermal management functionalities.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1891499</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1891499</link>
        <title><![CDATA[Role of carbon sequestration methods in enhancing water holding capacity of dredged Yellow River sediment: biochar and CO2 utilization]]></title>
        <pubdate>2026-07-20T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Min Zhang</author><author>Jinhua Feng</author><author>Dehui Guo</author><author>Yuting Fu</author><author>Shuze Xiao</author><author>Hua Yuan</author><author>Yunlu Hou</author>
        <description><![CDATA[Dredged Yellow River sediment (DYRS) is widespread in nature and generally features low water holding capacity due to poor grain grading and lack of clay minerals. Low water holding capacity can impede its application in interdisciplinary engineering and ecological scenarios such as ecological slope substrate and ecological remediation of mining area. This study investigates the role of carbon sequestration methods in the water holding capacity and microscopic mechanism of DYRS. DYRS is improved by two types of carbon sequestration methods, i.e., biochar additive and CO2 curing with the agent of reactive MgO (rMgO). The results show that the biochar additive and CO2 curing lead to an increase rate of water holding capacity by 49.5% and 180%, respectively. The biochar-treated DYRS features an optimum water holding capacity of DYRS, corresponding to an optimum particle size fraction of biochar. However, such an optimum water holding capacity of DYRS does not hold for the case of CO2 curing. The increasing dose of rMgO and CO2 curing duration are both favorable for improving the water holding capacity of DYRS, attributed to the binding products of chemical reaction. The performance of water holding capacity in treated DYRS is closely associated with altered pore structures by carbon sequestration methods. Biochar leads to a change of trimodal pore structure in untreated DYRS to bimodal pore structure in treated DYRS. However, CO2 curing reshapes the trimodal pore structure and facilitates the formation of new smaller pore sizes in treated DYRS. The research findings are fundamental for the future application of dredged river soils and carbon sequestration methods in engineering practice.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1919334</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1919334</link>
        <title><![CDATA[Editorial: Advanced materials and technologies for sustainable development of underground resources - volume II]]></title>
        <pubdate>2026-07-20T00:00:00Z</pubdate>
        <category>Editorial</category>
        <author>Jiangyu Wu</author><author>Weiqiang Chen</author><author>Hao Shi</author><author>Dan Ma</author><author>Hong S. Wong</author>
        <description></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1894197</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1894197</link>
        <title><![CDATA[Durability evaluation of cement-stabilized semi-rigid base courses incorporating recycled aggregates from steel slag, coal gangue, and construction waste]]></title>
        <pubdate>2026-07-16T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Rong Niu</author><author>Xu Wu</author><author>Jingzhuo Zhao</author><author>Bo Hu</author><author>Hongtao Qin</author><author>Junlin Zhang</author>
        <description><![CDATA[Steel slag (SS), coal gangue (CG), and construction waste (CW) were investigated as partial replacements in cement-stabilized aggregate mixtures for highway semi-rigid bases, with incorporation rates ranging from 0% to 80%. Performance assessments included unconfined compressive strength, flexural strength, drying shrinkage, and freeze-thaw resistance, followed by optimal material selection using a comprehensive fuzzy algorithm. Results indicated that SS synergistically enhanced overall performance. Active components within SS induced micro-expansion, reducing drying shrinkage by 29.5%–40.0%. Furthermore, continued hydration increased 360-day compressive strength by 16.0%–36.2%, flexural strength by 42.1%–52.9%, and the freeze-thaw strength ratio by 17.3%. Conversely, CW content exceeding 60% increased drying shrinkage by 10.8% due to fine aggregate hydration, yielding only marginal compressive strength gains (4.4%–7.3%) at 360 days. High CG levels (>40%) caused significant degradation in mechanical and durability properties due to layer structure disintegration; compressive strength decreased by 30.9%–46.9%, flexural strength fell by 40%, and freeze-thaw resistance declined by over 10%. Drying shrinkage for all mixtures conformed to the EXPASSOC model (R2 > 0.99), exhibiting a three-stage pattern where 85% of shrinkage occurred within 60 days, followed by stabilization after 100 days. A derived cracking resistance index confirmed that SS dosages of >40% provided optimal anti-cracking performance. Fuzzy comprehensive algorithm analysis identified SS (40%–80% incorporation) as the optimal material choice. Consequently, CG requires strict limitation to ≤40%, whereas CW is permissible at ≤ 40% (excluding fine aggregates). These findings provide theoretical support for the classified resource utilization of multi-source solid wastes in highway base courses.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1904975</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1904975</link>
        <title><![CDATA[Failure evolution and strength modeling of H-jointed layered sandstone under compression]]></title>
        <pubdate>2026-07-15T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Liqun Guo</author><author>Bo Li</author><author>Xu Chang</author>
        <description><![CDATA[BackgroundH-shaped joints, which consist of tensile and shear parts, are common in layered rocks and substantially affect rock failure and instability.ObjectiveTo explore the mechanical performances of the H-jointed sandstone under different loading conditions.MethodsUniaxial and confined compressive tests were carried out on H-jointed sandstone samples. The samples’ stress-strain responses, failure modes, AE activities, and strength were analyzed.ResultsThe results show that the stress-strain curve has four phases: crack closing, elastic phase, elastic-plastic phase, and residual stages. The failure patterns of the H-jointed samples change from tension to shear as the joint dip angle increases. Tensile failure is dominant at lower inclination angles, whereas shear slip failure occurs along the joint surfaces at higher angles. Sliding along the joint surfaces with tensile cracking is observed at moderate angles. The joint roughness coefficient (JRC) significantly influences the samples’ mechanical behavior. A modified Hoek-Brown criterion that considers the joint dip angle and JRC is suggested for evaluating the strength of H-jointed rock samples under compression.ConclusionsThis study provides a better understanding of the mechanical performance of H-jointed sandstone and a method to evaluate the strength.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1862791</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1862791</link>
        <title><![CDATA[Eco-friendly pavement raveling detection based on in-situ data and transfer learning]]></title>
        <pubdate>2026-07-14T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Juanjuan Wen</author><author>Yi Jiang</author><author>Yi Peng</author>
        <description><![CDATA[Pavement raveling is characterized by the progressive loss of surface aggregates and poses significant challenges to road durability and safety. The early detection and monitoring of this disease are crucial for implementing timely maintenance interventions. This study adopts a transfer learning approach for automated raveling detection in asphalt pavements. A comprehensive in situ raveling dataset comprising 530 images and 215 normal pavement images was collected using the LS-40 portable three-dimensional surface analyzer. Following histogram equalization for noise reduction, the dataset was augmented to 1600 images through mirroring and rotation techniques. The transfer learning was fine-tuned on four base convolutional neural network structures: the VGG16, the EfficientNet-B0, the InceptionV3, and the RegNet. The models were trained using standardized parameters, including an input size of 224 × 224, a batch size of 32, and 200 epochs, with regularization and dropout techniques applied to mitigate overfitting. A comparative analysis of optimization algorithms showed that RMSprop outperformed both SGD and Adam for this specific task. Transfer learning significantly enhanced the performance of all models, with the EfficientNet-B0 achieving outstanding results—achieving both high accuracy (99.7%) and low energy consumption in raveling detection. The selected models achieved AUC values exceeding 0.95, while the transfer learning significantly reduced training time and enhanced feature extraction capabilities, as confirmed through convolutional layer visualization. These findings establish the EfficientNet-B0 as the optimal structure for practical deployment in automated pavement inspection systems, providing a robust foundation for intelligent infrastructure maintenance strategies.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1698212</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1698212</link>
        <title><![CDATA[A simplex-centroid designed eco-friendly acetate-based deicer: development, environmental assessment, and evaluation of its anti-icing performance]]></title>
        <pubdate>2026-07-10T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Jinlong Guo</author><author>Wenjuan Zhao</author><author>Tao Wu</author><author>Shujun Wang</author><author>Bin Sun</author><author>Manbin Yang</author><author>Tengfei Yao</author><author>Bo Li</author>
        <description><![CDATA[Road icing in winter very easily poses a threat to driving safety. The application of road snow melting agent can improve this problem, but current road snow melting agents pose a threat to the environment and road infrastructure. The purpose of this study is to prepare a low-carbon, environmentally friendly road snow melting agent and explore its performance. In this study, low-carbon salts were selected as raw materials, and the components of low-carbon environmentally friendly snow melting agents were optimized by simplex center-of-gravity design. Then, the indoor and outdoor ice-melting performance and environmental protection performance of low-carbon environmentally friendly road snow melting agent were studied. Finally, the low-carbon environmentally friendly snow melting agent was incorporated into the asphalt mixture to prepare a low-carbon, environmentally friendly anti-icing asphalt mixture, and its anti-icing performance was evaluated. The results showed that a large concentration of low-carbon environmentally friendly road snow melting agent had an inhibitory effect on the corrosion of carbon steel, and the effect of such an agent on plant seeds was smaller than that of traditional chlorine salt road snow melting agent. The low-carbon, environmentally friendly anti-condensation ice asphalt mixture showed good anti-condensation ice performance; in particular, the anti-condensation ice asphalt mixture prepared by external mixing method shows more obvious anti-condensation ice performance. The optimum ratio of low-carbon, environmentally friendly road snow melting agent is 23.9% potassium acetate, 27.4% sodium acetate, and 48.7% ammonium acetate.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1858512</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1858512</link>
        <title><![CDATA[Experimental study on the mechanism and active prevention and control of crystalline clogging in tunnel drainage systems in limestone areas]]></title>
        <pubdate>2026-07-07T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Biao Shu</author><author>Chenglin Du</author><author>Xinxian Li</author><author>Wen Nie</author><author>Haobin Cui</author><author>Jia Li</author><author>Bo Chen</author>
        <description><![CDATA[The tunnel drainage system in limestone areas is highly susceptible to calcium carbonate crystallization clogging, which abnormally increases pore water pressure and threatens structural safety. Although traditional passive dredging methods are widely used, there is a critical research gap regarding the dynamic evaluation of complex material interventions under active flowing karst water. To elucidate the internal clogging mechanism and propose an “active prevention” material-source control strategy, this study combined on-site sampling from the Hubeishan Tunnel of the Guangzhou-Shenzhen Expressway with large-scale dynamic physical model simulations under single-factor controlled conditions. The results demonstrate that: (1) The clogging material is predominantly calcite (>98% purity), originating from the continuous leaching of free calcium in highly alkaline shotcrete. (2) The accelerator exhibits a nonlinear regulatory effect; a 10% dosage serves as the optimal independent threshold to prevent severe calcium leaching caused by micro-defects at higher dosages. (3) For water reducers, a 5% dosage is identified as the optimal independent threshold, whereas increasing the dosage to 10% triggers a severe crystallization outbreak, indicating the highest clogging risk. (4) Fly ash demonstrates a robust linear inhibitory effect on crystallization accumulation, with a 20% dosage acting as its optimal independent threshold. Furthermore, aggressive highly mineralized water (e.g., NaHCO3-type) directly skips atmospheric CO2 diffusion, rapidly reacting with leached calcium and exponentially accelerating the clogging process. These findings shift the engineering paradigm from passive mitigation to active source interception, providing critical quantitative references for suppressing early-stage calcium leaching and laying a theoretical foundation for future multi-factor orthogonal mix design in deep-buried karst tunnels.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1869575</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1869575</link>
        <title><![CDATA[Suppression of torsional fatigue cracking in a 35CrMo planetary carrier by QPQ treatment]]></title>
        <pubdate>2026-07-07T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Yong Ma</author><author>Jiangang Zhang</author><author>Qingbi Zhao</author><author>Shengdun Zhao</author><author>Fan Li</author>
        <description><![CDATA[A 35CrMo planetary carrier used in a hybrid transmission system was found to crack at the window region during torsional fatigue testing, threatening component durability and service reliability. To identify the failure origin and improve crack resistance without changing the component geometry or substrate material, static torsion testing, fracture observation, finite element stress analysis, surface characterization, comparative process evaluation, and component-level fatigue verification were carried out. The static torsion test yielded a torque of 5310 N·m, much higher than the applied fatigue load of ±2200 N·m, indicating that the failure was unlikely to be caused by gross overload. Fractographic observations revealed brittle features, including intergranular and cleavage fracture, suggesting surface-controlled crack initiation in the local high-stress window region. Compared with atmosphere nitriding, QPQ treatment produced a denser and more continuous compound layer mainly composed of ζ-Fe2N and Fe3O4, with a white-layer thickness of about 17.6 μm. The surface hardness increased to 785 HV1, and dry sliding tests showed lower friction fluctuation and a narrower wear scar width. Fatigue verification showed no cracking in QPQ-treated planetary carriers, demonstrating that QPQ treatment can effectively reduce crack-initiation tendency and improve the service reliability of 35CrMo planetary carriers.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1872779</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1872779</link>
        <title><![CDATA[Effects of RCA and ITS on the performance of cement-stabilized macadam]]></title>
        <pubdate>2026-07-02T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Xin Lu</author><author>Jingjing Huang</author><author>Yaogang Tian</author><author>Xiaohui Yan</author><author>Jing Jiang</author><author>Chunlin Yang</author><author>Jun Zhang</author>
        <description><![CDATA[To explore the resource utilization approaches of construction solid waste, this study partially replaced natural crushed stones with recycled coarse aggregates (RCAs) (0%, 30%, 50%, and 70%) and used iron tailings sand (ITS) replace part of the natural sand (0%, 25%, 50%, and 75%) in the preparation of cement-stabilized macadam (CSM). Through unconfined compressive strength, flexural tensile strength, dry shrinkage, and temperature shrinkage tests, the mechanical properties and shrinkage characteristics were systematically analyzed. The results indicate that with increasing RCA dosage, the strength of the CSM exhibits a downward trend, but the incorporation of ITS can effectively improve its mechanical properties. Multi-scale experiments show that 50% ITS has the best synergistic effect. ITS mitigates the defects caused by RCAs through micro-filling and particle interlocking, reducing interface microcracks by 40%, and forming a continuous interface transition zone (ITZ). At the microstructure level, flaky ITS particles refine the pores, delay strain failure, and promote ductile behavior. This research provides a scientific basis for infrastructure recovery through the high-value utilization of waste materials and tailings.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1900366</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1900366</link>
        <title><![CDATA[Editorial: Advancing eco-friendly construction: the role of biomass and waste integration]]></title>
        <pubdate>2026-07-01T00:00:00Z</pubdate>
        <category>Editorial</category>
        <author>Jue Li</author><author>Chen Chen</author><author>Miao Yu</author>
        <description></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1857441</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1857441</link>
        <title><![CDATA[Natural rubber modified asphalt with dynamic disulfide bonds and hydrogen bonds: rheological behavior and self-healing performance]]></title>
        <pubdate>2026-07-01T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Xiaoyu Yu</author><author>Xuejuan Cao</author><author>Tianqiang Jiang</author><author>Zhe Wu</author><author>Guilian Cao</author><author>Miao He</author>
        <description><![CDATA[Natural rubber-modified asphalt suffers from weak high-temperature deformation resistance and inferior self-healing capacity. To address these drawbacks, this work fabricates a novel self-healing rubber asphalt (CD-ENRA) via synergistic reinforcement of epoxidized natural rubber (ENR) and cellulose nanocrystal (CNC), combined with dynamic disulfide bond crosslinking. A bio-based composite modifier (C-ENR) was first synthesized with ENR and CNC as reinforcing fillers, followed by incorporation of a dynamic disulfide crosslinker (DTSA), and systematic characterizations were conducted to clarify how C-ENR and DTSA dosages affect the conventional pavement performance indicators, rheological behaviors, micromorphology, and self-repairing capability of CD-ENRA. At the optimal formulation of 5 wt% C-ENR and 0.75 wt% DTSA (denoted CD-ENRA-5), the softening point and ductility increased by 6.46% and 16.82%, respectively, compared with the DTSA-free counterpart C-ENRA-5, demonstrating superior high-temperature stability and low-temperature flexibility. At elevated temperatures, CD-ENRA-5 possessed the maximum crosslink density, which suppressed the slippage of asphalt molecular chains; consequently, it delivered the highest complex modulus and smallest phase angle across all specimens, alongside a 58.24% reduction in unrecoverable creep compliance, thereby greatly improving rutting resistance. For low-temperature service performance, CD-ENRA-3 (3 wt% C-ENR + 0.45 wt% DTSA) achieved the minimum complex modulus owing to its moderate crosslink density that maintained sufficient mobility of molecular segments, showing the best resistance to low-temperature cracking. Microscopic observations revealed that CNC constructed a sacrificial hydrogen-bond network to facilitate energy dissipation and realize homogeneous dispersion of the ENR matrix. Benefiting from the reversible dynamic disulfide bonds, CD-ENRA-5 exhibited prominent crack self-healing performance, with a healing index up to 67.5% after 35 min of healing treatment. Collectively, the incorporation of dynamic disulfide bonds simultaneously strengthens the high-temperature rheological performance, low-temperature toughness, and intrinsic self-healing property of ENR/CNC composite modified asphalt. The fabrication of high-performance, self-healing bio-based asphalt modifiers from renewable raw materials provides a promising strategy for advancing sustainable and eco-friendly pavement construction materials.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1845994</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1845994</link>
        <title><![CDATA[Experimental study on failure process of tailings dams under water infiltration and rainfall]]></title>
        <pubdate>2026-06-26T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Yixiong Gan</author><author>Wengang Liu</author><author>Bo Zhang</author><author>Ye Cheng</author><author>Wende Zhu</author><author>Weipeng Hao</author><author>Chen Wang</author>
        <description><![CDATA[IntroductionThis study investigated the failure mechanisms of tailings dams through centrifuge model tests using a multifunctional geotechnical centrifuge.MethodsSpecialized infiltration devices and rainfall simulation systems were developed for the centrifugal environment to examine dam behavior under both water seepage and rainfall conditions. The research systematically analyzed the failure evolution process while comprehensively evaluating multiple response parameters including water level, pore pressure, earth pressure, and displacement during deformation and failure.ResultsThe experimental results demonstrate that under water infiltration conditions, with settlement initiating at the crest at 700 s, on the slope surface at 900 s, and at the toe at 1000 s. And higher stacking height leads to larger settlement. Significant pore pressure buildup near the dam crest leads to progressive cracking and eventual global sliding failure. Rainfall conditions produce distinct failure characteristics featuring surface erosion coupled with rapid pore pressure increases, resulting in auniform surface erosion rather than deep-seated progressive failure Furthermore, the study established a quantitative model relating loading rate to stability and proposed a four-stage early warning thresholds (stable: <2.6, initial deformation: 2.6–5.6, accelerated development: 5.6–13.1, failure: ≥13.1 m/year) based on the observed evolutionary patterns, providing valuable guidance for safe construction practices.DiscussionThese findings offer important insights into tailings dam failure mechanisms under different environmental conditions, with significant implications for disaster prevention in similar geotechnical engineering projects.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1816072</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1816072</link>
        <title><![CDATA[On the detection of re-entrant features from metal additively manufactured samples and their correlations with manufacturing parameters]]></title>
        <pubdate>2026-06-23T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Tomasz Bartkowiak</author><author>Michał Jakubowicz</author><author>Patryk Mietliński</author><author>Michał Wieczorowski</author>
        <description><![CDATA[Metal additive manufacturing (AM), particularly laser powder bed fusion (L-PBF), often yields complex surface topographies that include re-entrant features—undercut geometries that cannot be detected or quantified using conventional surface metrology based on single-valued height functions. These features influence key functional properties such as wettability, fatigue strength, and tribological behavior, and may also serve as indicators of sub-optimal processing conditions. In this work, we present a systematic methodology for the detection and quantification of re-entrant features from cross-sectional profiles obtained via high-resolution X-ray micro-computed tomography (microCT). Titanium alloy samples (Ti-6Al-4V) were manufactured using 20 combinations of laser power and scanning speed. From each reconstructed volume, profiles were extracted and analyzed using a geometric algorithm based on B-spline form fitting and projection tracking. Two quantitative metrics were introduced to describe the share of re-entrant features with respect to both the total profile length and its fitted form. Statistical evaluation using two-way ANOVA revealed that laser power has a significant effect on re-entrant feature intensity (p < 0.05), whereas scanning speed showed no meaningful influence within the tested range. Linear regression confirmed a strong correlation (R2 > 0.9) between both metrics and laser power. The results demonstrate that insufficient energy input promotes the formation of re-entrant geometries through incomplete melting and particle bonding. The proposed method enables quantitative assessment of complex AM surface features that are inaccessible to traditional instruments, offering a pathway toward improved process control, surface quality evaluation, and functional performance optimization in metal AM. The geometry-based nature of the method suggests its applicability to a broader range of materials and additive manufacturing processes, provided appropriate imaging resolution is achieved.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1831858</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1831858</link>
        <title><![CDATA[Reaction mechanisms of the hydration products of solidified sulfate saline soils in the long-term solid waste period]]></title>
        <pubdate>2026-06-16T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Chongyang Wang</author><author>Jingwei Gong</author><author>Chong Shi</author><author>Miaomiao Gong</author><author>Zeshi Ren</author>
        <description><![CDATA[To ensure effective utilization of saline soils in cold and arid areas as engineering materials, we used calcium carbide slag along with slag, slag + fly ash, and fly ash as the cementitious materials to solidify sulfate saline soil. We then studied the effects of the salt content, calcium carbide slag content, and aging period on the compressive strengths of solidified soil samples containing different compositions of the active cementitious materials. The hydration products of the solidified soil samples were characterized under different conditions by X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, thermogravimetric analysis, and mercury intrusion porosimetry. The results of these analyses showed thast the salt and calcium carbide slag contents significantly affected the strengths of the solidified soil samples. When the salt content was 3.1% and calcium carbide slag content was 7%, the synergistic effects were found to be maximal in the solidified soil system containing different active cementitious materials. Moreover, under high salt content and a lengthy aging period, we found that stronger activities of the cementitious materials were not linked to higher strengths of the solidified soil samples. Through experimental evaluations, we found that the influence of high salt content on the solidified soil was reflected in changes in the amounts of hydration products formed and the corresponding pore structure.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1813690</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1813690</link>
        <title><![CDATA[Effect of fly ash and metakaolin on early-age autogenous shrinkage and mechanical properties of ultra-high-performance concrete]]></title>
        <pubdate>2026-06-15T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Yutai Liu</author><author>Ruiqing Hao</author><author>Lin Liao</author><author>Jinchang Zhao</author><author>Zhiling Liao</author><author>Zebiao Hou</author><author>Mingji Ding</author>
        <description><![CDATA[To address the severe autogenous shrinkage and high cracking risk caused by the extremely low water-to-binder ratio in traditional ultra-high-performance concrete (UHPC), this study incorporates fly ash (FA, 10%, 20%, and 30%) and metakaolin (MK, 5%, 10%, and 15%) individually, as well as in binary blending (20% total replacement), as partial cement replacements in UHPC production. All specimens were subjected to standard room-temperature curing conditions (20 °C ± 2 °C). The effects and underlying mechanisms of FA and MK on the rheological properties, mechanical properties, shrinkage behavior, and microstructure of UHPC were systematically investigated. The results of experiments and microscopic analysis (XRD and SEM) indicate that while the incorporation of FA reduces the mechanical properties slightly, it significantly enhances the rheological performance and effectively mitigates early-age autogenous shrinkage of UHPC. On the other hand, although the addition of MK impairs both the rheological and mechanical properties of UHPC slightly, it notably compensates for autogenous shrinkage deformation. With a binary blend of 20% (10% FA and 10% MK), the 28 days compressive strength of UHPC was 85.5% that of the control group, the tensile strength increased by 3.3%, and early-age autogenous shrinkage decreased by 28.4%. Although MK reduces the rheology due to its competitive water consumption with cement particles, the micro-expansion products generated by its highly reactive components, as confirmed by XRD and SEM analyses, significantly alleviate autogenous shrinkage. This study provides an effective strategy for autogenous shrinkage control in UHPC.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1715897</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1715897</link>
        <title><![CDATA[Sand shape effect on the hydraulic conductivity and compressibility of clay sand liners]]></title>
        <pubdate>2026-06-12T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Muawia Dafalla</author><author>Abdullah A. Shaker</author>
        <description><![CDATA[Designing environmental protection barriers requires careful consideration in the choice of coastal sand material used in clay-sand mixtures. The purpose of this study is to present a comparison and guide between two methodologies to investigate sands of different nature and shapes for the hydraulic conductivity and compressibility. Hydraulic conductivity is generally measured using the falling head test, which was carried out in a cell with a rigid lateral wall and one-dimensional water flow. The flexible wall method is another approach that simulates the natural field conditions. ASTM D5084 and BS1337-6:1990 were found appropriate to provide reliable hydraulic conductivity values. The differences in hydraulic conductivity measurements are expressed in terms of orders of magnitude. A flexible wall, falling head permeameter unit in which lateral confinement can be controlled and changed, was utilized for this study. The flow was found to assume different passages with enlarged tracks when confinement is relaxed. The sphericity of the sand grains used in this study indicated a 0.860 for rounded grains and 0.642 for the angular grains. The tests conducted enabled comparison of compressibility and geotechnical parameters for the clay sand mixtures, including sand of different shapes and angularity. The differences obtained for the hydraulic properties are influenced by the grain size and shape. Predicted hydraulic conductivity and compressibility depends to a greater extent on the shape and sand texture. The obtained results can be used as a predictive guide to liner performance and field applications.]]></description>
      </item><item>
        <guid isPermaLink="true">https://www.frontiersin.org/articles/10.3389/fmats.2026.1836853</guid>
        <link>https://www.frontiersin.org/articles/10.3389/fmats.2026.1836853</link>
        <title><![CDATA[The effect of treatment way of wash water form ready-mixed concrete plant on the properties of mortar]]></title>
        <pubdate>2026-06-11T00:00:00Z</pubdate>
        <category>Original Research</category>
        <author>Haitao Zhou</author><author>Xianwei Ma</author><author>Xiao Wang</author><author>Feng jian Zhang</author><author>Lanzhen Yu</author>
        <description><![CDATA[The settling time of wash water from a ready-mixed concrete plant in a tank will affect its solid content and ion concentrations, which will further influence the properties of new concrete mixed using that wash water. However, the effects of settling time and ion concentration have received scant attention. A method of simulating wash water formation in a ready-mixed concrete plant was provided in this article. Different settling times were designed, and a retarding component (RC) was added to change the solid content and ionic concentrations. The fluidity, strength, and hydration of mortar mixed with wash water were studied. The results show that a long wash water settling time can improve the strength of mortar, but the RC will increase the solid content and reduce the ion concentrations in the wash water. As a result, a longer settling time is required. In a word, a suitable wash water settling time is beneficial to mortar properties.]]></description>
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