ORIGINAL RESEARCH article

Front. Earth Sci., 06 January 2026

Sec. Economic Geology

Volume 13 - 2025 | https://doi.org/10.3389/feart.2025.1701181

Fractal characteristics of full-scale pores and throats in tight sandstone and their application in the analysis of the main controlling factors of a reservoir

  • Natural Gas Research Institute of Yanchang Petroleum (Group) Co. LTD, Xi’an, China

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Abstract

Comprehensive and accurate characterization of pore–throat structures is essential for rational resource assessments and enhanced recovery rates in tight sandstone reservoirs. However, the fractal characteristics of full-scale pores and throats in tight sandstones remain poorly understood. In this study, high-pressure mercury intrusion (HPMI), constant-rate mercury intrusion (CRMI), and nuclear magnetic resonance (NMR) experiments are integrated to provide a full-scale characterization of pore and throat distributions in tight sandstone samples. Fractal dimensions are calculated separately for pores and throats using a wetting-phase model and a 3D capillary tube model. Based on these results, seven pore–throat systems are identified: 1) small bundle-like throats within clay interstitial filler, 2) medium tubular/sheet throats generated by intense compaction, 3) large throats formed by localized dilation of tubular/sheet throats, 4) micropores created by localized constriction of submicron–micron sized intergranular pores, 5) small pores dominated by intragranular dissolution pores, 6) medium pores consisting mainly of residual intergranular pores, and 7) large pores resulting from the combination of moldic pores and residual intergranular pores. Moreover, the reservoir space exhibits a ternary structural characteristic. Both small and medium throats conform to the capillary tube assumption, with mean fractal dimensions of 2.2093 and 2.7214, respectively. Small, medium, and large pores fit the spherical assumption, with mean fractal dimensions of 2.8180, 2.7435, and 2.9825, respectively. Extensive overlap between large throats and micropores forms a beaded pore–throat network for which an appropriate fractal model is currently lacking. The porosity and permeability of the samples in this study are primarily controlled by medium pores and medium throats, followed by small pores, while movable fluid resides predominantly within medium pores. The results suggest that relatively weak compaction is a key factor in the development of high-quality reservoirs in the strata studied. The proposed full-scale classification scheme based on fractal dimensions offers new insights into the microscopic heterogeneity of tight sandstones. Furthermore, the full-scale characterization combined with correlation analysis and pore–throat genesis discrimination provides targeted strategies for exploration of high-quality, tight sandstone reservoirs.

1 Introduction

The pore–throat structure is a key factor influencing reservoir storage capacity and flow behavior (Wang J. et al., 2024), and it controls both hydrocarbon occurrence and development efficiency (Dou et al., 2021; Wu Y. et al., 2022; Wang et al., 2024c). In tight sandstone reservoirs, intense diagenesis, particularly compaction, profoundly alters the pore–throat network (Liu et al., 2024; Wang et al., 2024c; Yang Y. et al., 2024), resulting in a broad size distribution (Wang J. et al., 2021; Wu Y. et al., 2022) that is dominated by nano-to micro-scale features (He et al., 2024; Wang J. et al., 2024). This network displays irregular morphology (Wang et al., 2024b), limited connectivity (He et al., 2024; Liu et al., 2024; Wang et al., 2024c; Yang Y. et al., 2024) and pronounced heterogeneity (Wu Y. et al., 2022; He et al., 2024; Liu et al., 2024; Wang et al., 2024c), all of which complicate hydrocarbon grading evaluation (Xie et al., 2023) and impede enhanced recovery rates (Xiao et al., 2016; Xin et al., 2022; Xu et al., 2022; He et al., 2024). Consequently, accurate and comprehensive characterization of pore–throat structure has become a central focus of tight sandstone research worldwide (Xie et al., 2023; He et al., 2024; Wang et al., 2024b). Previous studies have examined pore throats through Euclidean geometry, fractal theory, and topological analysis (Wu et al., 2019). The present work emphasizes fractal characterization grounded in Euclidean representations.

Euclidean geometric descriptors of pore throats encompass their morphology, absolute dimensions, and size-frequency distributions. Currently, two principal categories of characterization techniques have been established: direct methods based on image analysis, represented by scanning electron microscopy (SEM), atomic force microscope (AFM), and X-ray computed tomography (X-CT), and indirect methods based on fluid injection or physical radiation parameter conversion, exemplified by experiments such as high-pressure mercury intrusion (HPMI), constant-rate mercury intrusion (CRMI), nuclear magnetic resonance (NMR), NMR cryoporometry (NMR-C), N2 gas adsorption (N2GA), CO2 gas adsorption (CO2GA) and small-angle x-ray scattering (SAXS) (Wu et al., 2019; Wu Y. et al., 2022; Yang et al., 2023; He et al., 2024; Liu et al., 2024; Wang J. et al., 2024; Wang et al., 2024c; Yang M. et al., 2024; Zhu et al., 2025). No single technique, however, spans the entire nano–micro–milli scale of pore throat diameters (Pan et al., 2021; Qiao et al., 2022; Yang et al., 2023; Wang et al., 2024c), nor can most techniques reliably distinguish pores from throats. Hence, combined approaches that leverage complementary detection ranges and models are increasingly adopted (Qiao et al., 2022; He et al., 2024; Wang et al., 2024b; Wang et al., 2024c). In such schemes, calibrated NMR T2 spectra typically represent pore radius distributions from submicron to millimeter scales (Wu Y. et al., 2022; Liu et al., 2024; Wang et al., 2024c); HPMI, NMR-C, or N2GA resolve nano-scale pore throats (Wu et al., 2019; He et al., 2024); CO2GA and SAXS target ultrafine pore throats (<2 nm) (Wang J. et al., 2024); while discrimination between pores and throats relies on CRMI (Xiao et al., 2016; Wang F. et al., 2021; Wang et al., 2024c; Wu Y. et al., 2022) or high-resolution X-CT (Zhang et al., 2020).

Fractal theory has established the self-similar nature of rock pore–throat systems (Katz and Thompson, 1985; Krohn, 1988), with the fractal dimension (Df) serving as a robust quantitative indicator of microscopic reservoir heterogeneity (Wu Y. et al., 2022; Xu et al., 2022; Zang et al., 2022; Yang et al., 2023; Wang J. et al., 2024; Wang et al., 2024b; Wang et al., 2024c). In recent years, numerous researchers have applied fractal theory to the microscopic study of reservoirs, developing calculation models tailored to various pore–throat characterization techniques (Wang F. et al., 2018; Zhang et al., 2024). Extensive correlation analyses have been conducted between fractal dimensions and rock components (Han et al., 2023), reservoir quality (Cheng et al., 2023; Wang et al., 2024c), and pore–throat parameters (Nan et al., 2023; He et al., 2024; Liu et al., 2025). These efforts have established a conceptual bridge linking pore–throat structure to macroscopic petrophysical properties and sedimentary diagenetic environments. Empirical evidence indicates that fractal behavior varies across scales within pore–throat networks, yielding distinct Df values from the nano-to-millimeter domains (Wang J. et al., 2021; Qiao et al., 2022; Zhao et al., 2023; Wang et al., 2024b). Some scholars have attempted to explain these scale-dependent variations by extending basic geometric models and proposing classification schemes for pore–throat systems. For instance, Zhu et al. (2019) attributed these variations to pore–throat morphology, dividing pore–throat systems into tubular and bead-like types. Wang et al. (2023), by contrast, linked Df differences to the suitability of fractal computation models, classifying pore–throat models as the shuttlecock model and the spiny ball model.

However, conventional methods for deriving fractal dimensions of pore–throat systems in tight sandstones have typically relied on discrete calculations based on isolated experimental datasets (Zhang et al., 2019; Guo et al., 2020; Pan et al., 2021; Qiao et al., 2022; Wang Z. et al., 2020; Wang J. et al., 2021; Wu Y. et al., 2022; Xin et al., 2022; Xu et al., 2022; Zang et al., 2022). Such fragmented methodology often obscures the continuous, scale-dependent nature of pore–throat fractal behavior and limits the ability to capture the full complexity of the system (Wang X. et al., 2018; Guo et al., 2019). Moreover, existing studies have not conducted full-scale fractal analyses that independently quantify pores and throats using geometry-appropriate models while clearly distinguishing between the two (Qiao et al., 2020; Qu et al., 2020; Wang W. et al., 2020).

To address these gaps, this work integrates HPMI, CRMI, and NMR into a continuous, full-scale characterization framework for pore–throat networks in tight sandstones. Fractal dimensions are calculated separately for pores and throats, and pore–throat systems across multiple scales are delineated, thereby providing new insights into microscopic heterogeneity. Finally, by correlating pore–throat genetic types with reservoir quality, the principal controls on reservoir performance are identified.

2 Materials and methods

2.1 Geological setting and samples

A total of 46 core plugs with standard dimensions of 2.54 cm diameter and 5.5 cm length were used in this study. All samples were collected from the Middle Jurassic tight sandstone in a basin of western China, with the sampling area shown in Figure 1A. All cores consist of channel sandstones deposited in a meandering river system (Figure 1B), at burial depths of 1,970–2,600 m. During the Yanshanian tectonic period, the region underwent episodes of uplift and subsidence, leading to limited fracture development. As a result, all samples analyzed in this study are free of natural fractures.

FIGURE 1

Map and diagram illustrating geological data. Panel A shows a map of China with Beijing marked by a star and a study area highlighted in a square. Panel B presents a stratigraphic column for the Jurassic period, detailing lithology with alternating layers of sand, mud, and shale. Thickness ranges from 450 to 1500 meters, indicating sedimentary facies and tectonic movements like meandering river facies and uplift and subsidence linked to the Yanshan movement. A legend identifies symbols used.

Geological overview of the study area. (A) Location of the sampling area and (B) sedimentary facies and tectonic movement characteristics of the target interval.

2.2 Experimental measurements

Figure 2 depicts the experimental workflow applied to each core plug. Two wafers, 0.5 cm and 1.0 cm in thickness, were cut from the plug top; the thinner wafer was processed into casting thin sections (CTS) while the thicker wafer was used for scanning electron microscopy (SEM). The remaining plug was then subjected to non-destructive measurements of porosity, permeability, saturated-state NMR, and high-speed centrifugation (HSC). Following these tests, the plug was bisected into two specimens of approximately 2.5 cm: one for HPMI and the other for CRMI. Because all measurements are from the same original plug, the resulting datasets are fully paired and directly comparable.

FIGURE 2

Flowchart depicting a cylindrical sample undergoing various experimental measurements. Initially, the sample is tested for CTS and SEM. It is then assessed for porosity, permeability, and NMR (saturation). Post-cutting, two smaller cylindrical samples are used for further measurements: HSC leads to HPIM, and the smaller sample leads to CRMI. Experimental measurements and sample status are labeled at the top.

Experimental scheme of single core plug.

2.2.1 CTS and SEM

For CTS analysis, samples were ground to a thickness of approximately 30 μm, impregnated with blue epoxy resin, and examined under a polarizing microscope. During this step, pore morphologies were characterized, genetic classifications determined, and pore radii estimated.

For SEM analysis, samples were fractured, sputter-coated with gold, and imaged using an FEI Quanta-200F field-emission SEM. This procedure emphasized throat morphology and genetic classification, which are features that can be indistinct under optical microscopy, and provided approximate measurements of throat radii.

2.2.2 Porosity and permeability testing

Porosity and permeability were measured using a PoroPDP-200 helium-porosimeter/permeameter (Core Lab, USA). Prior to testing, all core plugs were dried at 110 °C for 24 h to remove residual fluids. Porosity was calculated from helium-expansion measurements using Boyle’s law. Permeability was determined by an unsteady-state gas-flow method and corrected for gas slippage (Klinkenberg effect).

2.2.3 NMR and HSC

Each plug was weighed dry (m0), evacuated under vacuum for 18 h, and subsequently saturated with degassed deionized water under a confining pressure of 20 MPa for 72 h. The saturated weight (m1) was recorded immediately after removal. T2 spectra were acquired at 32 °C using a low-field NMR analyzer (NMRC12-010V, Newmai, China) with echo spacing of 0.1 ms, an echo count of 9,000, and a repetition time of 6,000 ms.

Following NMR measurement, plugs were subjected to high-speed centrifugation at 14,000 rpm (≈6.5 MPa displacement pressure) for 1 h to expel movable fluids; afterward, the post-centrifugation weight (m2) was recorded. Movable water saturation (Swm) was calculated as Equation 1

2.2.4 HPMI and CRMI

Specimens were oven-dried at 110 °C for 24 h to remove residual moisture. HPMI was performed on an AutoPore IV 9505 analyzer (Micromeritics, USA), and CRMI was performed on an ASPE 730 system (Coretest, USA).

Mercury, as a non-wetting fluid, requires external pressure to invade pore–throat constrictions. Assuming cylindrical capillaries, intrusion pressure (Pc) and throat radius (r) obey the Washburn equation (Washburn, 1921):where Pc is in MPa, σ is the surface tension (mN/m), θ is the contact angle (°), and r is the throat radius (µm).

During HPMI, the maximum intrusion pressure reached 412 MPa, with mercury’s contact angle at 140° and surface tension at 480 mN/m, according to Equation 2, it corresponds to a minimum detectable capillary radius of approximately 2 nm. Prior studies show that throat constrictions behave as cylindrical capillaries, whereas pores exhibit considerably larger radii and irregular geometries. As mercury progresses from throats into pores, capillary forces within the larger pores become negligible, producing a pore-shielding effect whereby HPMI-derived size distributions superimpose pore signals onto throat signals, thereby misrepresenting the true pore radii (Yao and Liu, 2012; Xiao et al., 2016; Zhu et al., 2019).

CRMI addresses this by injecting mercury at a constant low rate (0.00005 mL/min), exploiting the pressure differential between the throat and pore entry. In this study, the maximum CRMI pressure of 6.2 MPa corresponds to a minimum detectable throat radius of approximately 120 nm via the Washburn equation (Washburn, 1921). Because CRMI assumes ideal spherical pores, reported pore radii are equivalent-sphere values; when pores are connected to larger throats, the measured volume actually reflects the combined pore–throat networks, leading to overestimated pore radii. Therefore, only CRMI-derived throat radius data are employed in this study.

2.3 Methodology

2.3.1 Conversion between NMR T2 spectrum and radius distribution

NMR arises from the interaction between atomic nuclei and an external magnetic field (Meng et al., 2016). The transverse relaxation time (T2) measured in NMR experiments reflects both the amplitude and rate of relaxation of hydrogen nuclei within pores and throats of different sizes. The overall transverse relaxation rate is the sum of three contributions (Kleinberg and Horsfield, 1990; Coates et al., 1999):where T2 is the transverse relaxation time, ms; T2B is the bulk relaxation time, ms; is the surface relaxivity, μm/ms; S is the pore–throat surface area, μm2; V is the pore–throat volume, μm3; D is the diffusion coefficient, μm2/ms; γ is the gyromagnetic ratio, (T·ms)−1; G is the average magnetic field gradient, 10−4 T/cm; and TE is the echo spacing, ms.

For a rock sample saturated with a single fluid in a homogeneous magnetic field, and with sufficiently short echo spacing, both the bulk term and the diffusion term can be neglected (Kleinberg and Horsfield, 1990; Daigle and Johnson, 2016). Equation 3 then simplifies to

The surface-to-volume ratio (S/V) relates to pore geometry viawhere Fs is a shape factor: it equals 2 for cylindrical capillaries and 3 for spheres. Combining Equations 4, 5 yields

According to Equation 6, T2 is controlled by ρ and the reciprocal of V/S and is directly proportional to the pore–throat radius r. Thus, larger r values correspond to longer T2. In HPMI experiments, mercury initially overcomes lower capillary forces to invade larger pore throats, and subsequently, with increasing pressure, enters progressively smaller pore throats. Consequently, the cumulative summation of the normalized NMR signal in descending order of T2 produces a curve analogous to the capillary curve. By linearly fitting T2 against V/S for each intrusion-saturation step, the can obtained, from which pore–throat radii r can be calculated under either cylindrical or spherical assumptions. The specific surface area S is derived from HPMI data via Equation 7 (Xiao et al., 2016)

2.3.2 Fractal theory and models

Based on the experimental principles of HPMI, CRMI, and NMR, this study characterizes throat radius distributions using HPMI and CRMI data, assuming that throats behave as capillary tubes. Pore radius distributions are obtained from NMR data assuming spherical pores. Accordingly, the fractal models used to calculate fractal dimensions of pores and throats must conform to these geometric assumptions.

According to fractal theory (Mandelbrot et al., 1984), the self-similarity of storage space in tight sandstones is described by the relationship between the number of pore throats and their radii:where N (>r) is the number of pore throats with radius greater than r, dimensionless; rmax is the maximum radius, µm; f(r) is the probability density function of pore–throat radii; Df is the fractal dimension, dimensionless.

2.3.2.1 3D capillary tube model

The 3D capillary tube model assumes that the reservoir’s storage network comprises capillaries of varying radius and length, which is consistent with the morphological assumptions underlying HPMI and CRMI experiments. When computing the fractal dimension using HPMI and CRMI data, the 3D capillary model should therefore be employed. Because mercury preferentially invades larger capillaries, the cumulative intrusion volume can represent the volume of all throats with a radius exceeding r. Thus, the equivalent number of throats with radius >r is given by (Wang et al., 2018):where VHg is the cumulative intrusion volume, µm3, and l is the capillary length, µm. Equation 9 does not yield the actual throat count but the equivalent number of capillaries of radius r required to fill VHg. Combining Equations 8, 9 giveswhere DT is the throat fractal dimension (dimensionless). Equation 10 simplifies to

Li (2010) incorporated the Washburn equation to recast Equation 11 in terms of mercury saturation SHg and capillary pressure Pc:where a is a dimensionless constant. Taking logarithms of Equation 12, yields

Equation 13 describes a linear relationship in double-logarithmic space between mercury saturation SHg and capillary pressure Pc. Hence, the throat fractal dimension computed via the 3D capillary tube model relates to the slope K1 of this regression aswhere K1 is the slope of the fitted line under the 3D capillary tube model.

2.3.2.2 Wetting-phase model

The wetting-phase model applies to experiments using a wetting-phase fluid as the detection medium (Zhang et al., 2017), and it assumes that the rock’s storage space comprises spheres of radius r. In NMR experiments, deionized water serves as the detection medium. When the shape factor (Fs) is set to 3, the model accurately reflects the distribution of spherical pores, aligning with both the medium requirements and model assumptions of the wetting-phase model. Therefore, when calculating the fractal dimension from NMR data, the wetting-phase model should be selected. Because the wetting fluid preferentially occupies the smallest pores, the cumulative volume of pores with radii below r is (Huang et al., 2017):where V (<r) is the volume of pores <r, µm3; and rmin is the minimum pore radius, µm. From Equation 8, the probability density of pore radii is (Huang et al., 2017):where N (<r) is the count of pores <r and DP is the pore fractal dimension. Substituting Equations 15, 16 yields Equation 17.

The total pore volume iswhere rmax is the maximum pore radius, µm. Thus, According to Equation 17, wetting-phase saturation Sw becomes

For rmaxrmin, Equation 19 simplifies to Equation 20

Then, taking logarithms gives

Equation 21 describes a linear relationship, in double-logarithmic coordinates, between the wetting-phase and r. Accordingly, the pore fractal dimension calculated from the wetting-phase model relates to the slope of the linear regression line as follows:where K2 is the slope of the fitted line under the wetting-phase model.

3 Results

3.1 Petrophysical properties

Table 1 summarizes porosity, permeability, and movable water saturation for all 46 core plugs, which are labeled A1–A46 in descending porosity. Porosity spans 3.32–15.90% (mean 10.04%, median 9.98%), permeability spans 0.002–38.230 mD (mean 2.218 mD, median 0.181 mD), and movable water saturation is 8.84%–70.68% (mean 44.26%, median 50.75%). Figure 3 demonstrates a strong positive correlation between porosity and permeability (R2 = 0.8446) and shows that movable water saturation increases systematically with both porosity and permeability. Given the relatively strong correlations among porosity, permeability, and movable fluid saturation, the reservoirs represented by the samples were classified into four types, primarily based on porosity, in descending order of quality: type I (>13%), type II (10%–13%), type III (7%–10%), and type IV (<7%) (Table 1).

TABLE 1

Sample Type φ (%) K (mD) S m (%) Sample Type φ (%) K (mD) S m (%)
A1 15.90 38.230 53.95 A24 9.92 0.183 56.93
A2 15.81 5.121 58.47 A25 9.73 0.085 29.00
A3 15.09 3.689 48.08 A26 9.58 0.308 52.95
A4 14.94 3.180 56.50 A27 8.95 0.057 27.40
A5 14.43 25.455 67.68 A28 8.64 0.055 14.65
A6 14.40 5.049 59.88 A29 8.58 0.092 48.12
A7 14.21 0.412 45.36 A30 8.53 0.117 30.43
A8 14.01 1.306 62.43 A31 8.24 0.092 27.98
A9 13.79 0.630 53.27 A32 8.15 0.051 54.70
A10 13.23 0.997 56.47 A33 7.89 0.036 14.78
A11 13.18 7.515 61.40 A34 7.77 0.107 63.03
A12 12.96 5.401 67.82 A35 7.49 0.031 49.42
A13 12.59 0.247 50.80 A36 7.46 0.031 39.39
A14 12.27 0.263 70.68 A37 7.27 0.055 11.21
A15 12.21 0.176 49.07 A38 7.25 0.036 10.54
A16 12.18 0.521 58.89 A39 6.87 0.029 51.64
A17 11.93 0.409 60.50 A40 6.45 0.020 32.77
A18 11.54 0.345 48.95 A41 5.73 0.018 9.72
A19 10.90 0.148 49.80 A42 4.67 0.009 8.84
A20 10.48 0.714 63.85 A43 4.57 0.053 38.54
A21 10.17 0.317 70.65 A44 4.52 0.002 14.32
A22 10.15 0.256 53.79 A45 3.95 0.009 21.84
A23 10.05 0.180 44.57 A46 3.32 0.003 15.04

Sample physical parameter statistics.

φ, porosity, K, permeability, Swm, movable fluid saturation.

FIGURE 3

Scatter plot showing the relationship between porosity and permeability. Data points are colored by movable fluid saturation percentage. The exponential trend line equation is y=0.0005e^0.5935x with R^2=0.8446. Permeability ranges from 10^-3 to 10^2 mD, porosity from 0% to 18%, and saturation from 0% to 80%.

Relationship between porosity, permeability, and movable fluid saturation.

3.2 Pore and throat types

CTS analysis reveals two principal pore types: residual intergranular pores and secondary dissolution pores. Residual intergranular pores persist between framework grains after compaction and cementation, bounded by relatively straight grain margins, with radii of 20–60 µm (Figure 4A). The visual cement content of samples is below 5%, indicating that compaction is the dominant controlling factor for the development of residual intergranular pores. Secondary dissolution pores include intragranular dissolution pores, which are honeycomb-like voids along feldspar cleavage planes, irregular in shape and 5–15 µm in radius (Figure 4B), and larger but rarer moldic pores formed by complete feldspar removal, which may exceed 100 µm in radius and locally interconnect (Figure 4C).

FIGURE 4

Microscopic images A to F show various pore structures in rock samples. Image A highlights residual intergranular pores. Image B shows intragranular pores. Image C displays moldic pores. Image D identifies necked throats. Image E features tubular and sheet throats. Image F illustrates bundle-like throats. Each image includes labeled arrows pointing to highlighted features.

Typical pore and throat types of samples. (A) Residual intergranular pore, sample A8, CTS. (B) Intragranular pore, sample A6, CTS. (C) Moldic pore, sample A21, CTS. (D) Constricted neck-shaped throat, sample 38, CTS. (E) Plate-like throat, sample 31, SEM. (F) Tube bundle throat, sample 29, SEM.

CTS and SEM observations identify three primary throat morphologies: necked, tubular/sheet, and bundle-like. Necked throats result from localized grain-boundary constrictions and measure 1–2 µm in radius (Figure 4D) but occur infrequently. Under strong compaction, tighter grain contacts produce tubular or sheet throats: cylindrical or ellipsoidal throats with radii <1 µm (Figure 4E). Finally, clay interstitial filler domains host abundant bundle-like throats with radii mostly below 0.1 µm (Figure 4F).

3.3 Pore–throat distribution based on single methods

Due to differences in instrument resolution, the raw sampling intervals of HPMI, CRMI, and NMR vary significantly: HPMI yields relatively sparse data points, while CRMI and NMR produce much denser measurements. These discrepancies hinder direct comparison, concatenation, and cross-method computation. To resolve this, CRMI and NMR data were resampled to match the HPMI interval, ensuring that all three techniques generate radius distribution curves with uniform spacing. This standardization enables valid comparison and provides a consistent basis for subsequent curve integration and analysis.

3.3.1 HPMI result

Figures 5A,C,E,G present the capillary pressure curves for each sample. Samples with higher reservoir quality exhibit a broader, gentler plateau at lower mercury saturation and an overall concave-downward shape. As reservoir quality declines, the plateau shortens, the slope steepens, and the curve trends toward a steeper, near-linear form. Final mercury saturations range from 49.64% to 98.44% and do not have a clear correlation with porosity or permeability (Table 2).

FIGURE 5

Graphs A to H show mercury intrusion porosimetry data for different samples. Each graph presents either pressure versus mercury saturation or frequency versus pore radius, depicted with lines in varying colors corresponding to specific sample groups: red, orange, green, and blue. Each pair of graphs (A-B, C-D, E-F, G-H) represents the same sample set.

Capillary pressure curve and reservoir space radius distribution of the samples. (A) and (B) Type Ⅰ. (C) and (D) Type II. (E) and (F) Type Ⅲ. (G) and (H) Type Ⅳ.

TABLE 2

Sample r max
(μm)
r peak (μm) r 50 (μm) (μm) S Hg (%) Sample r max
(μm)
r peak (μm) r 50 (μm) (μm) S Hg (%)
A1 7.555 6.479 1.822 3.043 91.39 A24 1.030 0.612 0.179 0.355 77.24
A2 4.525 3.480 0.389 1.396 81.91 A25 0.767 0.612 0.024 0.246 69.10
A3 3.016 0.771 0.316 0.866 87.81 A26 1.031 0.765 0.158 0.363 79.03
A4 2.388 1.890 0.496 0.921 83.93 A27 0.610 0.406 0.104 0.220 78.01
A5 7.555 5.333 1.259 2.766 90.09 A28 0.612 0.457 0.117 0.231 80.80
A6 5.333 4.524 0.808 1.734 85.15 A29 0.508 0.284 0.117 0.191 79.95
A7 1.611 1.032 0.265 0.414 98.44 A30 0.767 0.509 0.044 0.240 77.37
A8 3.771 3.481 0.327 1.238 76.75 A31 0.326 0.182 0.110 0.127 89.06
A9 1.558 1.030 0.271 0.561 85.01 A32 0.768 0.285 0.208 0.233 87.92
A10 2.409 1.030 0.170 0.759 68.63 A33 0.509 0.406 0.037 0.167 70.02
A11 3.771 3.232 0.647 1.491 86.99 A34 0.765 0.365 0.132 0.256 74.09
A12 2.107 1.562 0.513 0.679 96.56 A35 0.509 0.284 0.176 0.187 92.38
A13 1.023 0.762 0.270 0.365 90.89 A36 0.407 0.285 0.054 0.163 72.65
A14 1.562 1.562 0.098 0.521 71.87 A37 0.611 0.509 0.065 0.229 81.32
A15 0.768 0.612 0.286 0.346 90.06 A38 0.767 0.509 0.026 0.363 79.03
A16 1.564 0.768 0.180 0.464 80.21 A39 0.406 0.202 0.101 0.137 89.52
A17 1.564 0.767 0.270 0.514 77.11 A40 0.285 0.004 0.020 0.080 77.32
A18 1.032 0.612 0.336 0.367 88.52 A41 0.509 0.365 0.179 49.64
A19 1.030 0.508 0.166 0.321 83.21 A42 0.285 0.202 0.019 0.085 79.80
A20 1.032 0.767 0.169 0.394 72.31 A43 0.325 0.202 0.051 0.113 83.59
A21 1.557 0.612 0.324 0.464 83.90 A44 0.227 0.165 0.016 0.077 73.58
A22 1.335 0.768 0.335 0.421 85.04 A45 0.365 0.285 0.014 0.121 59.09
A23 1.033 0.766 0.128 0.376 78.39 A46 0.253 0.048 0.010 0.080 56.41

Pore–throat parameters based on HPMI.

r max, maximum radius; rpeak, peak radius; r50, median radius; , mean radius; SHg, final mercury saturation.

Figures 5B,D,F,H display the pore–throat radius distribution curves based on HPMI, with key size parameters summarized in Table 2. Maximum throat radii range from 0.227 μm to 7.555 μm, peak radii range from 0.004 μm to 6.479 μm, median radii range from 0.010 μm to 1.822 μm, and mean radii range from 0.077 μm to 3.043 μm. As reservoir quality deteriorates, the distributions narrow and shift systematically toward smaller radii.

3.3.2 CRMI result

Figure 6 presents representative capillary pressure curves for pores, throats, and the overall sample. Mercury intrusion proceeds through three distinct stages. In Stage 1 (the “pore stage”), the pore capillary pressure curve coincides with the overall curve, indicating that at low pressure, mercury invades the largest pore bodies first. During this stage, increases in mercury saturation are attributable entirely to pore filling, with no contribution from throats. In Stage 2 (the “pore–throat stage”), the throat capillary pressure curve rises sharply while the pore curve levels off, showing that at intermediate pressures, mercury begins to enter throats and saturation increases are governed primarily by throat filling, even though both pores and throats develop within a relatively narrow range of radii. In Stage 3 (the “throat stage”), the pore capillary pressure curve flattens completely while the throat curve rises slowly, signifying that mercury no longer enters pores but continues to fill throats. All further saturation increases are due to throat invasion, involving only the very small radii.

FIGURE 6

Two plots labeled A and B show mercury saturation versus pressure, in megapascals. Each plot depicts three curves: throat (blue), pore (orange), and total (red), representing different stages of mercury saturation. Both plots are divided into pore stage, pore-throat stage, and throat stage. Plot A ranges from 0 to 60 percent, and plot B from 0 to 45 percent saturation. Both plots illustrate how saturation changes with pressure, highlighting different dynamics for throat and pore contributions.

Pore, throat, and total capillary pressure curves of typical samples based on CRMI. (A) Sample A20 and (B) sample A43.

Figure 7 shows the throat radius distribution curves after resampling based on CRMI, with key throat size parameters summarized in Table 3. Maximum throat radii range from 0.325 µm to 4.522 µm, and peak radii range from 0.130 µm to 1.027 µm. Because CRMI is limited in capturing the full throat size spectrum, median and mean throat radii are not reported. As reservoir quality declines, the distributions of throat radius narrow and shift toward smaller values.

FIGURE 7

Line graphs labeled A, B, C, and D show frequency percentages against radius in micrometers. Graph A uses red tones for samples A1-A11, B uses orange for A12-A23, C uses green for A24-A38, and D uses blue for A39-A46. Each graph displays multiple overlapping lines.

Throat radius distribution of samples after resampling based on CRMI: (A) Type Ⅰ, (B) Type II, (C) Type Ⅲ, and (D) Type Ⅳ.

TABLE 3

Sample r max (μm) r peak (μm) Sample r max (μm) r peak (μm)
A1 3.772 0.769 A24 1.030 0.508
A2 1.333 0.509 A25 0.767 0.509
A3 2.789 0.771 A26 1.031 0.767
A4 2.112 0.613 A27 0.766 0.325
A5 3.016 1.027 A28 0.768 0.509
A6 1.567 0.767 A29 0.764 0.284
A7 0.766 0.509 A30 1.030 0.509
A8 2.129 0.771 A31 0.511 0.285
A9 1.558 0.612 A32 0.768 0.130
A10 1.332 0.612 A33 0.326 0.130
A11 4.522 0.767 A34 0.765 0.253
A12 2.107 0.612 A35 0.766 0.509
A13 0.762 0.507 A36 0.771 0.510
A14 2.753 0.767 A37 1.031 0.509
A15 0.768 0.509 A38 1.337 0.767
A16 1.030 0.284 A39 0.768 0.285
A17 2.113 0.767 A40 0.767 0.285
A18 0.612 0.285 A41 0.611 0.365
A19 1.030 0.130 A42 1.033 0.130
A20 1.032 0.130 A43 0.764 0.506
A21 1.027 0.509 A44 0.325 0.227
A22 0.768 0.285 A45 0.768 0.509
A23 1.335 0.612 A46 0.457 0.130

Throat-size parameters based on CRMI.

rmax, maximum radius; rpeak, peak radius.

3.3.3 NMR results

Figures 8A,C,E,G display the NMR T2 spectra for all samples, each exhibiting a bimodal pattern with a dominant short-T2 peak. This short-T2 peak reflects the abundance of small pore throats. As reservoir quality decreases, both the short- and long-T2 peaks shift toward shorter relaxation times, while the short-T2 peak becomes increasingly pronounced, indicating an increasing fraction of small pore throats and an overall reduction in pore throat size.

FIGURE 8

Graphs A to H show data variations for different samples. A and B depict frequency versus time and radius in red. C and D in yellow, E and F in green, G and H in blue. Each graph shows overlapping curves for multiple samples with corresponding legends indicating sample numbers.

NMR T2 spectra and reservoir space radius distribution after relaxation rate calibration and resampling (Fs = 2). (A) and (B) Type Ⅰ. (C) and (D) Type II. (E) and (F), Type Ⅲ. (G) and (H) Type Ⅳ.

Figures 8B,D,F,H present the corresponding pore–throat radius distribution curves, obtained by calibrating the T2 spectra using surface relaxivity and resampling to match the mercury intrusion interval, with a shape factor of 2 assumed for integration with HPMI and CRMI data. Key parameters are summarized in Table 4: calibrated relaxivities range from 0.039 μm/ms to 0.411 μm/ms; pore–throat radii span minimum values of 0.002–0.227 μm, maximum values of 6.477–218.088 μm, medians of 0.065–11.328 μm, and means of 0.224–23.998 μm. The resampled distributions remain bimodal, with the radii of the left peak at 0.048 μm–1.037 μm and of the right peak at 0.365–60.107 μm. With declining reservoir quality, these distributions progressively shift toward smaller radii.

TABLE 4

Sample (μs/ms) r min
(μm)
r max
(μm)
r 50 (μm) (μm) Sample (μs/ms) r min
(μm)
r max
(μm)
r 50 (μm) (μm)
A1 0.273 0.227 218.088 11.328 23.998 A24 0.081 0.013 113.297 0.457 3.653
A2 0.145 0.113 45.245 1.333 7.063 A25 0.092 0.015 36.305 0.202 1.287
A3 0.107 0.048 36.261 1.035 4.854 A26 0.095 0.032 36.302 0.406 2.585
A4 0.132 0.101 90.973 1.337 8.423 A27 0.125 0.019 113.207 0.253 1.904
A5 0.177 0.091 147.245 6.476 15.139 A28 0.113 0.002 91.010 0.285 1.746
A6 0.137 0.065 90.973 1.030 7.456 A29 0.075 0.015 113.575 0.253 2.738
A7 0.126 0.065 45.280 0.612 3.546 A30 0.066 0.004 146.967 0.227 2.375
A8 0.118 0.038 59.857 1.576 5.804 A31 0.061 0.019 60.060 0.182 1.381
A9 0.154 0.130 59.903 0.767 4.737 A32 0.082 0.027 113.107 0.406 3.771
A10 0.067 0.038 36.277 0.612 3.325 A33 0.175 0.011 217.511 0.165 2.494
A11 0.175 0.065 174.750 3.232 10.572 A34 0.059 0.027 36.276 0.325 2.659
A12 0.135 0.065 113.581 1.885 8.512 A35 0.099 0.027 147.236 0.325 3.453
A13 0.093 0.038 91.019 0.762 7.098 A36 0.053 0.011 36.277 0.165 1.901
A14 0.039 0.013 45.261 0.365 2.389 A37 0.411 0.019 216.900 0.284 3.026
A15 0.094 0.027 36.299 0.509 3.220 A38 0.199 0.010 174.869 0.182 3.710
A16 0.059 0.027 36.269 0.612 3.093 A39 0.057 0.017 113.073 0.202 3.771
A17 0.106 0.113 45.284 0.612 4.647 A40 0.052 0.005 60.018 0.091 0.849
A18 0.096 0.038 60.026 0.769 5.048 A41 0.241 0.004 175.973 0.130 1.792
A19 0.073 0.032 36.267 0.406 3.380 A42 0.154 0.003 113.009 0.101 1.766
A20 0.044 0.022 36.250 0.508 3.357 A43 0.063 0.011 91.261 0.151 1.882
A21 0.054 0.032 45.259 1.888 6.523 A44 0.134 0.004 147.600 0.091 2.789
A22 0.118 0.038 60.079 0.612 5.070 A45 0.072 0.005 60.119 0.091 1.869
A23 0.115 0.038 45.197 0.406 3.191 A46 0.044 0.004 6.477 0.065 0.224

Pore–throat parameters based on NMR T2 spectra calibrated by relaxation rate.

, relaxation rate; rmin, minimum radius; rmax, maximum radius; rpeak-L, peak radius of the left peak; rpeak-R, peak radius of the right peak; r50, median radius; , average radius; SHg, final mercury saturation.

3.4 Full-scale pores and throats distribution based on multiple methods

The HPMI, CRMI, and NMR results for the same sample were plotted on a unified coordinate system (Figures 9A,D,G). The radius distribution curves from the three methods exhibit overlapping peaks, and the left-side shapes of the pore–throat based on HPMI and the throat distributions based on CRMI coincide closely. These agreements confirm both the reliability of the matched HPMI and CRMI data and the accuracy of the NMR relaxivity calibration.

FIGURE 9

Nine graphs labeled A to I display frequency percentage versus radius in micrometers for samples A1, A12, and A23. Different colored lines represent NMR results, HPIMI results, CRM results, full-scale capillary throats, and full-scale spherical pores. The data varies across samples, showing different frequency distributions and peaks in each graph.

Full-scale capillary throat and spherical pore characterization results of typical samples. (A–C) Sample A1. (D–F) Sample A12. (G–I) Sample A23.

CRMI results demonstrate that only throats occur below a radius of 0.12 μm. Accordingly, in the HPMI distribution, all radii <0.12 μm are attributed to throats. Because both HPMI and CRMI assume capillary tube geometry for throats, their curves can be spliced at 0.12 μm to yield a continuous, full-scale capillary tube throat distribution (Figures 9B,E,H).

The pore–throat distribution based on NMR (with shape factor Fs = 2) can then be directly compared and integrated with this full-scale throat distribution curve. In Figures 8B,E,H, the lower limit of the throat distribution falls below the NMR detection threshold, and in some ranges, the throat proportion exceeds the total pore–throat proportion. This indicates that NMR underrepresents nanometer-scale pore throats because their relaxation times decay too rapidly, faster than the first echo can be sampled. Consequently, only NMR data to the right of the intersection with the full-scale throat curve are used in this study. Subtracting the full-scale throat distribution curve from these NMR data yields the full-scale capillary tube pore distribution, which is then converted to a full-scale spherical pore distribution by multiplying by the geometry conversion factor 3/2 (Figures 9C,F,I).

The main size parameters for the full-scale throats and pores are presented in Tables 5 and 6. Throat radii range from 0.002 μm to 0.009 μm (minimum) to 0.325–3.772 μm (maximum), with median values of 0.020–0.257 μm and mean values of 0.056–0.562 μm. Pore radii satisfy rmaxrmin, with minimum radii of 0.019–0.765 μm, maximum radii of 11.334 μm–624.502 μm, median radii of 0.080–31.670 μm, and mean radii of 0.569–52.871 μm. The pore size characteristics agree well with CTS observations, and the throat-size characteristics align with SEM observations, confirming that the combined HPMI-CRMI-NMR approach provides a realistic description of pore and throat size distributions in tight sandstones.

TABLE 5

Sample r min
(μm)
r max
(μm)
r 50 (μm) (μm) Sample r min
(μm)
r max
(μm)
r 50 (μm) (μm)
A1 0.004 3.772 0.257 0.562 A24 0.002 1.030 0.087 0.188
A2 0.002 1.333 0.147 0.255 A25 0.002 0.768 0.090 0.167
A3 0.002 2.789 0.210 0.443 A26 0.004 1.031 0.100 0.240
A4 0.003 2.112 0.082 0.246 A27 0.002 0.766 0.056 0.139
A5 0.005 3.016 0.195 0.552 A28 0.002 0.768 0.123 0.185
A6 0.002 1.567 0.120 0.250 A29 0.002 0.764 0.103 0.139
A7 0.003 0.766 0.054 0.160 A30 0.002 1.030 0.050 0.149
A8 0.003 2.130 0.255 0.387 A31 0.003 0.511 0.057 0.115
A9 0.002 1.558 0.110 0.247 A32 0.004 0.768 0.080 0.133
A10 0.003 1.332 0.181 0.274 A33 0.002 0.326 0.047 0.083
A11 0.003 3.4803 0.180 0.473 A34 0.004 0.765 0.100 0.146
A12 0.004 2.107 0.072 0.217 A35 0.003 0.766 0.099 0.167
A13 0.003 0.762 0.062 0.167 A36 0.003 0.771 0.104 0.182
A14 0.004 2.753 0.141 0.310 A37 0.003 1.031 0.096 0.210
A15 0.002 0.768 0.096 0.174 A38 0.002 1.337 0.034 0.168
A16 0.002 1.030 0.057 0.166 A39 0.003 0.768 0.059 0.142
A17 0.004 2.113 0.200 0.375 A40 0.002 0.767 0.039 0.118
A18 0.004 0.612 0.081 0.141 A41 0.002 0.611 0.119 0.174
A19 0.004 1.030 0.045 0.143 A42 0.002 1.034 0.024 0.056
A20 0.003 1.032 0.101 0.168 A43 0.002 0.764 0.020 0.097
A21 0.009 1.027 0.125 0.198 A44 0.002 0.325 0.020 0.058
A22 0.003 0.768 0.050 0.147 A45 0.003 0.769 0.048 0.136
A23 0.003 1.335 0.097 0.198 A46 0.004 0.457 0.046 0.087

Size parameters of full-scale throats.

rmin, minimum radius; rmax, maximum radius; r50, median radius; —average radius.

TABLE 6

Sample r min
(μm)
r max
(μm)
r 50 (μm) (μm) Sample r min
(μm)
r max
(μm)
r 50 (μm) (μm)
A1 0.765 624.502 31.670 52.872 A24 0.057 169.945 3.710 8.190
A2 0.303 67.868 7.536 14.214 A25 0.040 425.165 0.369 4.708
A3 0.248 54.391 8.101 11.967 A26 0.072 220.754 1.760 5.903
A4 0.248 425.100 7.930 17.196 A27 0.057 324.022 0.642 4.676
A5 0.170 424.286 18.207 30.709 A28 0.057 90.119 0.930 5.854
A6 0.151 325.115 8.574 16.217 A29 0.033 170.363 1.070 7.185
A7 0.151 67.920 1.503 7.790 A30 0.057 262.113 0.608 6.447
A8 0.072 424.389 7.038 13.372 A31 0.057 90.090 0.807 4.252
A9 0.303 612.208 1.464 14.131 A32 0.072 169.661 3.073 7.837
A10 0.072 261.832 4.640 7.274 A33 0.057 326.267 0.459 7.926
A11 0.136 613.064 13.728 27.615 A34 0.049 261.815 2.179 6.690
A12 0.303 427.711 10.449 18.917 A35 0.057 263.220 2.919 9.439
A13 0.097 263.525 6.254 16.133 A36 0.033 136.381 0.675 4.207
A14 0.033 263.305 2.776 6.358 A37 0.072 325.350 0.349 11.876
A15 0.151 54.448 1.902 7.397 A38 0.057 262.304 0.287 9.474
A16 0.072 262.807 4.448 7.501 A39 0.057 169.609 1.762 6.429
A17 0.272 430.136 4.725 10.902 A40 0.028 90.028 0.173 2.391
A18 0.136 324.998 5.457 11.041 A41 0.026 263.959 0.171 3.808
A19 0.072 169.584 3.568 7.748 A42 0.040 169.514 0.176 4.922
A20 0.040 136.148 3.321 7.193 A43 0.033 136.892 0.265 4.324
A21 0.072 67.888 7.628 13.780 A44 0.028 263.915 0.158 7.626
A22 0.072 423.953 4.497 11.803 A45 0.028 90.178 0.172 4.190
A23 0.097 262.043 2.250 9.442 A46 0.019 11.334 0.080 0.569

Size parameters of full-scale pores.

rmin, minimum radius; rmax, maximum radius; r50, median radius; , average radius.

3.5 Full-scale fractal characteristics of pores and throats

The fractal dimensions of throats were calculated using the 3D capillary tube model (Equations 13 and 14). In double-logarithmic plots of lg Pc versus lg SHg, the regression curves exhibit three distinct segments at the slope changes, partitioning the throat network into small, medium, and large throats (Figures 10A–C). Pore fractal dimensions were derived from the wetting-phase model (Equation 22). Similarly, four segments appear in plots of lg r versus lg Sw, delineating micropores, small pores, medium pores, and large pores (Figures 10D–F).

FIGURE 10

Graphs A to F display pore-throat size distributions across different samples. The x-axis shows logarithmic pore or capillary pressure (lg P_c), and the y-axis shows logarithmic saturation (lg S_Hg or lg S_w). Data points are color-coded by pore-throat sizes: small, medium, large throats, and micro, small, medium, large pores. Each graph presents linear equations with R-squared and fractal dimension values, demonstrating different sample characteristics.

(A–C) Full-scale throat fractal characteristics of samples A1, A12, and A23 (D–F). Full-scale pore fractal characteristics of samples A1, A12, and A23.

The fractal dimensions for each class are listed in Table 7 (throats) and Table 8 (pores), with the corresponding radius ranges shown in Figure 11. In double-logarithmic space, the coefficients of determination for the throat types range from 0.8202 to 0.9917, and for the pore types from 0.8049 to 0.9985, most exceeding 0.9000, demonstrating robust classification. Small throats, with radii of 0.002 μm–0.122 μm (predominantly <0.100 μm), exhibit fractal dimensions DT1 between 2.1168 and 2.3923 (mean 2.2093). Medium throats span 0.100–2.299 μm (mainly 0.100–0.560 μm) and have DT2 between 2.4098 and 2.9393 (mean 2.7214). Large throats range from 0.140 μm to 3.772 μm (mostly 0.345–1.300 μm) with DT3 between 4.8913 and 9.5803 (mean 6.2768). Micropores extend from 0.019 μm to 3.961 μm (predominantly 0.030–1.000 μm) and yield DP1 between 0.2040 and 1.9816 (mean 1.3778). Small pores (1.000–5.430 μm) have DP2 between 2.4182 and 2.9902.

TABLE 7

Sample D T1 R2 D T2 R2 D T3 R2 Sample D T1 R2 D T2 R2 D T3 R2
A1 2.1239 0.9428 2.7171 0.9532 5.7756 0.9036 A24 2.1946 0.9548 2.6571 0.9651 6.2978 0.9669
A2 2.1324 0.8407 2.6714 0.9518 4.8913 0.9848 A25 2.1642 0.978 2.687 0.9333 5.6649 0.9599
A3 2.117 0.8737 2.5349 0.9361 6.5113 0.9234 A26 2.2175 0.9484 2.4098 0.9062 5.3761 0.9749
A4 2.2042 0.8758 2.6469 0.927 6.0948 0.9056 A27 2.2046 0.9226 2.6614 0.962 6.8577 0.9152
A5 2.231 0.9737 2.4828 0.912 6.7934 0.9468 A28 2.1395 0.9112 2.8137 0.9626 7.0865 0.9588
A6 2.1674 0.9195 2.6832 0.9396 7.6002 0.9139 A29 2.1833 0.9709 2.8935 0.9657 6.1252 0.9318
A7 2.2391 0.8971 2.6827 0.9217 5.9254 0.9864 A30 2.1879 0.8545 2.7548 0.9311 6.7758 0.9764
A8 2.1223 0.9581 2.5026 0.9335 5.2182 0.9419 A31 2.2334 0.9096 2.9255 0.9727 7.9443 0.8805
A9 2.1599 0.9021 2.6007 0.9543 5.5856 0.9399 A32 2.2549 0.9758 2.9339 0.9654 6.0437 0.9144
A10 2.1168 0.9215 2.6675 0.9556 5.3681 0.9831 A33 2.1906 0.827 2.9393 0.9675 6.5574 0.9621
A11 2.16 0.9594 2.7161 0.9508 5.1389 0.918 A34 2.2268 0.958 2.8242 0.9769 5.6667 0.9688
A12 2.2485 0.9417 2.8036 0.9464 5.9816 0.8828 A35 2.1937 0.9513 2.7401 0.9624 6.4343 0.9205
A13 2.2146 0.9471 2.6431 0.9445 5.4143 0.9682 A36 2.2003 0.9526 2.5953 0.9409 5.5594 0.9675
A14 2.1887 0.958 2.8503 0.9653 5.2473 0.9585 A37 2.2107 0.9835 2.4617 0.9056 5.9371 0.9053
A15 2.1678 0.9421 2.7608 0.9323 5.7199 0.9721 A38 2.2498 0.9372 2.6751 0.9548 4.9328 0.979
A16 2.2043 0.8974 2.8539 0.9289 5.2762 0.9917 A39 2.2289 0.9328 2.742 0.9446 6.0805 0.9479
A17 2.1493 0.9699 2.5678 0.9437 6.2835 0.8828 A40 2.2565 0.9757 2.9071 0.9266 6.6774 0.9531
A18 2.2334 0.9517 2.805 0.9573 6.5475 0.9464 A41 2.1711 0.9822 2.4949 0.9518 7.4992 0.9076
A19 2.2994 0.9691 2.695 0.9737 7.0082 0.9257 A42 2.2786 0.9595 2.8571 0.9748 7.8953 0.8803
A20 2.1728 0.9093 2.8411 0.9756 6.0742 0.9551 A43 2.37 0.9836 2.7322 0.9216 6.0878 0.9774
A21 2.2425 0.9509 2.7587 0.9597 6.2079 0.9706 A44 2.3923 0.97 2.9036 0.9672 9.5803 0.8399
A22 2.245 0.9725 2.7606 0.9526 5.5897 0.9746 A45 2.2532 0.9409 2.7601 0.9393 8.9852 0.8202
A23 2.1839 0.9144 2.7333 0.9768 6.5828 0.9403 A46 2.3003 0.9408 2.8378 0.9657 5.8324 0.953

Multi-scale fractal dimension of the throat system.

D T1, fractal dimension of small throat; DT2, fractal dimension of medium throat; DT3, fractal dimension of large throat.

TABLE 8

Sample D P1 R2 D P2 R2 D P3 R2 D P4 R2 Sample D P1 R2 D P2 R2 D P3 R2 D P4 R2
A1 0.7864 0.9233 2.4182 0.9964 2.3177 0.9839 2.9651 0.8319 A24 1.298 0.9623 2.7982 0.9811 2.6921 0.9469 2.9879 0.9530
A2 0.8010 0.8913 2.7962 0.9876 2.5919 0.9919 2.8701 0.9607 A25 0.9085 0.8178 2.8795 0.8953 2.8422 0.9746 2.9946 0.9665
A3 0.6201 0.9163 2.6857 0.955 2.4468 0.9939 2.9397 0.9451 A26 1.1471 0.9469 2.7625 0.9797 2.7398 0.9635 2.9962 0.9482
A4 0.9116 0.9106 2.8201 0.9765 2.6580 0.9842 2.9982 0.9586 A27 1.7693 0.8873 2.8994 0.9917 2.9066 0.9866 2.9943 0.9032
A5 0.3999 0.9336 2.7657 0.9723 2.5321 0.9647 2.9985 0.9155 A28 2.0055 0.9409 2.9147 0.9606 2.9061 0.9883 2.9635 0.9118
A6 1.1305 0.9310 2.8887 0.9468 2.6401 0.9791 2.9961 0.9891 A29 1.8059 0.8454 2.8429 0.9742 2.7781 0.9673 2.9785 0.8818
A7 1.7007 0.9146 2.8372 0.9787 2.7542 0.9985 2.964 0.9189 A30 1.9816 0.9269 2.8345 0.9928 2.8244 0.9465 2.9848 0.9231
A8 1.7962 0.9123 2.8194 0.9216 2.5894 0.9576 2.9958 0.9831 A31 1.9715 0.8655 2.8050 0.9722 2.8161 0.9508 2.9900 0.9650
A9 0.7746 0.8534 2.9892 0.8496 2.7496 0.9538 2.9916 0.9402 A32 1.8681 0.9269 2.7070 0.991 2.7050 0.9480 2.9801 0.9169
A10 0.5813 0.9137 2.7779 0.9430 2.6774 0.9491 2.9982 0.9501 A33 2.0289 0.9401 2.9883 0.8799 2.9399 0.9933 2.9893 0.9552
A11 0.8786 0.9101 2.7475 0.9620 2.5232 0.9424 2.9916 0.8773 A34 1.8349 0.8171 2.8007 0.9843 2.7429 0.9782 2.9958 0.9540
A12 1.1602 0.9369 2.6754 0.9899 2.5926 0.9771 2.9971 0.9725 A35 1.8800 0.8426 2.7573 0.9967 2.7872 0.9371 2.9915 0.9296
A13 1.6408 0.8381 2.7362 0.9910 2.7120 0.9839 2.997 0.8892 A36 1.9038 0.8930 2.8494 0.9867 2.8191 0.9616 2.9963 0.9019
A14 1.6606 0.8054 2.7920 0.9829 2.7409 0.9360 2.9978 0.8222 A37 1.8308 0.8416 2.9768 0.8200 2.9417 0.9927 2.9818 0.9774
A15 1.2036 0.9570 2.8605 0.9911 2.6979 0.9922 2.9785 0.8990 A38 1.8674 0.8914 2.9426 0.8441 2.9270 0.9846 2.9803 0.9322
A16 1.2854 0.9408 2.7203 0.9907 2.6372 0.9554 2.9955 0.9566 A39 2.0287 0.9392 2.7664 0.9910 2.7779 0.9507 2.9862 0.8949
A17 0.2040 0.9033 2.8923 0.8672 2.6953 0.9589 2.9953 0.9667 A40 1.6025 0.8518 2.6911 0.9956 2.9203 0.9934 2.9765 0.9527
A18 1.5809 0.8891 2.8061 0.9828 2.6888 0.9537 2.9988 0.9801 A41 1.8604 0.8221 2.9836 0.8561 2.9594 0.9695 2.9863 0.9671
A19 1.4639 0.9645 2.7362 0.9867 2.6876 0.9752 2.9971 0.9424 A42 2.2129 0.8283 2.9902 0.8596 2.9608 0.9948 2.9933 0.9981
A20 1.2600 0.9320 2.7252 0.9966 2.6823 0.9719 2.9983 0.8676 A43 1.9311 0.8324 2.9246 0.9593 2.8691 0.9695 2.9885 0.9241
A21 0.7506 0.9137 2.5771 0.9839 2.5018 0.9958 2.8865 0.9658 A44 1.6032 0.8367 2.9849 0.8193 2.9661 0.9633 2.9942 0.9873
A22 1.7660 0.9528 2.8445 0.9908 2.7357 0.9621 2.9952 0.9593 A45 1.7394 0.8136 2.8816 0.8750 2.8662 0.9700 2.9423 0.9721
A23 1.3596 0.9020 2.7874 0.9876 2.7475 0.9706 2.991 0.9520 A46 1.3465 0.8049 2.9468 0.9838 2.9119 0.9920 2.9846 0.8559

Full-scale fractal dimension of the pore system.

D P1, fractal dimension of micropores; DP2, fractal dimension of small pores; DP3, fractal dimension of medium pores; DP4, fractal dimension of large pores (mean 2.8180). Medium pores (1.000–5.430 μm) have DP3 between 2.3177 and 2.9661 (mean 2.7435), and large pores (1.000–5.430 μm) exhibit DP4 between 2.8701 and 2.9988 (mean 2.9825).

FIGURE 11

Bar charts labeled A and B compare pore radius distributions across 50 samples. Chart A categorizes into small, medium, and large throats, while chart B includes micro, small, medium, and large pores. Both charts use a logarithmic scale for pore radius measurements, denoted in micrometers.

(A) Size distribution range of the throat system. (B) Size distribution range of the pore system.

In three dimensions, true fractal dimensions should lie between 2 and 3 (Zhang et al., 2017), with values closer to 2 indicating lower structural complexity and those closer to 3 reflecting higher complexity. The elevated DT3 for large throats and the low DP1 for micropores deviate from ideal fractal behavior. Notably, some DT3 significantly exceed the upper limit of 3, with maximum values approaching 10. Similarly, some DP1 fall far below 2, with maximum values approaching 0. These physically unrealistic values arise from the presence of throats with relatively large size but very low proportion and pores with relatively small size and significantly lower proportion within the samples. Such characteristics steepen the regression slope for data points corresponding to large throats and micropores. This pattern highlights pronounced heterogeneity in the development of large throats and micropores. Moreover, among throats, DT1 < DT2 indicates that medium throats are more complex than small ones; among pores, DP3 < DP2 < DP4 shows that large pores are most complex, followed by small pores, with medium pores the least complex.

4 Discussion

4.1 Genetic types and ternary structure of pore–throat systems

According to fractal theory, the fractal dimension of a reservoir pore–throat network reflects its geometric scaling: values near 2 correspond to two-dimensional proportional scaling, while those near 3 indicate three-dimensional proportional scaling (Li and Horne, 2006; Zhu et al., 2019; Wang et al., 2023). Dimensions below 2 or above 3 signify a significant departure from the assumed geometry: either a loss of self-similarity or the breakdown of the model.

For the capillary model of throats, the fractal dimension reflects how radius r and length l scale spatially. If r expands equally along two perpendicular axes, or if r and l both extend along a single axis with the same proportion, the throat undergoes two-dimensional proportional scaling (Df = 2). When r and l scale equally in all three dimensions, the throat exhibits three-dimensional proportional scaling (Df = 3) (Figure 12A). Intermediate or more complex scaling behaviors yield fractal dimensions between 2 and 3. Throughout these processes, throats remain cylindrical or ellipsoidal, preserving the capillary tube assumption. However, if throats interweave with adjacent pore bodies and undergo localized widening, their volume increases faster than predicted by the ideal model, and the fractal dimension exceeds 3.

FIGURE 12

Diagram comparing capillary-tube and spherical models, illustrating scaling transformations. Part A shows a capillary-tube model with two-way and three-way proportional extensions using cylinders, labeled with variables. Part B displays a spherical model with similar transformations using spheres. Both models include bead-string representations at the bottom, depicting scaling differences. Mathematical expressions accompany each model to show relationships.

Extended model of reservoir space. (A) Capillary tube model of throat (modified from Zhu et al., 2019), and (B) Spherical model of pores.

For the spherical model of pores, the fractal dimension reflects how the pore radius r scales in three-dimensional space. When r expands equally along all three axes, the pore undergoes three-dimensional proportional scaling (Df = 3); if r expands equally along only two axes, the pore exhibits two-dimensional proportional scaling (Df = 2) (Figure 12B). More complex or intermediate scaling behaviors yield Df values between 2 and 3. Throughout these processes, pore shapes remain roughly spherical or ellipsoidal, justifying the spherical pore assumption. However, if pores interpenetrate throats and undergo local necking, their volume contracts rapidly, causing the fractal dimension to drop below 2.

The radius distribution curves (Figure 11) reveal substantial size overlap between large throats and micropores. In this overlapping range, pores and throats interweave to form a beaded structure that is neither purely spherical nor strictly a capillary tube in geometry. Conventional techniques reliably distinguish large pores at the upper end and small throats at the lower end of the spectrum, but resolution diminishes where pore and throat sizes coincide. As a result, the 3D capillary tube model tends to overestimate fractal dimensions for large throats (Df > 3), while the wetting-phase model underestimates fractal dimensions for micropores (Df < 2).

Figure 13 illustrates the microfeatures and genetic origins of each pore–throat system using sample A1. Large pores consist of moldic pores combined with residual intergranular pores. In three-dimensional space, they approximate isotropic spheres (three-dimensional scaling), yielding fractal dimensions near 3. Medium pores are dominated by residual intergranular pores, which appear as elongated polygons in thin sections and flattened ellipsoids in 3D resemble (two-dimensional scaling), giving fractal dimensions near 2. Small pores, mainly fine intragranular dissolution pores, form a honeycomb pattern in thin sections, exhibiting more complex and irregular extension than medium pores, and thus higher fractal dimension. Micropores arise from locally necked submicron–micron-sized intergranular pores and display a beaded structure; under the spherical pore model, their fractal dimension falls below 2. Large throats originate from locally dilated tubular/sheet throats and likewise exhibit a beaded feature. Under the capillary tube model, their fractal dimension exceeds 3. Medium throats are mainly tubular or sheet, corresponding to the cylindrical or elliptical cylindrical shape in the extension process of the capillary tube model, whose extension falls between two- and three-dimensional proportional scaling, yielding fractal dimensions close to 2. Small throats, formed as orderly bundle-like tubes within clay interstitial filler, extend predominantly in two dimensions and thus conform to the capillary tube assumption, with fractal dimensions nearest 2.

FIGURE 13

Pore and throat characterization graph with frequency percentage on the vertical axis and pore/throat radius on the horizontal axis. Images depict various pore and throat types: micro, small, medium, large pores, and bundle-like, tubular, large throats. Visuals highlight localized constriction, intragranular dissolution, and moldic pores, with pore sizes ranging from 15 micrometers to 200 micrometers, and throat sizes from 10 micrometers to 100 micrometers. Data points on the graph are represented with colored circles.

Microscopic characteristics and genetic types of the pore–throat system of sample A1.

In summary, integrating fractal characteristics and genetic origins, the pore–throat network of tight sandstone can be partitioned into seven distinct types: (1) small bundle-like throats developed within clay interstitial filler, (2) medium tubular/sheet throats generated by intense compaction, (3) large throats formed by local dilation of tubular throats, (4) micropores created by localized constriction of submicron-micron sized intergranular pores, (5) small pores dominated by intragranular dissolution pores, (6) medium pores comprised mainly of residual intergranular pores, and (7) large pores resulting from the combination of moldic pores and residual intergranular pores. Morphologically, these seven types interlink to establish a complex reservoir structure composed of throats that conform to the extension characteristics of the capillary tube model, and beaded pore–throat assemblages and pores that fit the extension characteristics of the spherical model, together defining a ternary structural framework.

Previous studies on the fractal characteristics of tight sandstones have proposed various pore–throat classification schemes. For example, based on the 3D capillary tube model, Zhu et al. (2019) analyzed HPMI data, identifying two distinct pore systems: capillary tube pores, which are relatively small and exhibit ideal fractal dimensions, and beaded pores, which are larger and display fractal dimensions exceeding 3. Similarly, Wang et al. (2023) applied the equivalent-sphere model to interpret NMR data, categorizing pores into shuttlecock pores, which are smaller in size with ideal fractal behavior, and the spiny-spherical pores, which are larger and exhibit fractal dimensions greater than 3. However, these schemes are limited by their reliance on a single technique with restricted scale coverage, which hinders comprehensive fractal characterization across the full-scale pore–throat distribution. Moreover, the applied methods do not clearly differentiate between pores and throats, and they overlook differences arising from their underlying geometric models. In contrast, the classification scheme proposed in this study is based on full-scale fractal analyses that separately evaluate pores and throats. It applies different models tailored to their morphological characteristics, thereby addressing key limitations of previous approaches. Coupled with an analysis of the genetic differences among pore–throat systems, this scheme revealed the origin of the divergence in pore–throat fractal dimensions and offers a more rational and holistic perspective for understanding reservoir heterogeneity in tight sandstones.

Although the sample set employed in this study is limited in number, it encompasses a wide range of physical properties and pore–throat parameters. Reservoirs of varying quality consistently exhibit ternary pore–throat structures and similar multi-scale fractal behavior. Therefore, the findings presented here have some general applicability and can be extrapolated to reservoirs with comparable lithology in other regions.

4.2 Analysis of factors influencing reservoir quality based on the pore–throat fractal systems classification

In this study, pore–throat systems were first classified by fractal dimension, and then evaluated in terms of how the porosity contribution of each system correlates with total porosity, permeability, and movable fluid saturation. Each system’s genetic origin was also considered to assess its impact on reservoir quality.

All pore systems show positive correlations with reservoir quality parameters, but the contributions of large pores and micropores are essentially uncorrelated (R2 = 0.0043–0.2548; Figures 14A–C, J–L). Medium pores exhibit the strongest correlation (R2 = 0.7829–0.8269; Figures 14D–F), followed by small pores (R2 = 0.4520–0.6399; Figures 14G–I).

FIGURE 14

Twelve scatter plots labeled A through L, grouped by pore size: large (A-C), medium (D-F), small (G-I), and micro (J-L). Each plot shows relationships between porosity, permeability, and movable fluid saturation. Regression equations and R² values are provided for each trend line. Data points are color-coded by pore size: large (red), medium (orange), small (green), and micro (blue). Each plot includes an x-axis for porosity percentage and varying y-axes for total porosity, permeability, and movable fluid saturation.

Effect of the pore system on reservoir quality. (A) Porosity of large pores vs. total porosity, (B) porosity of large pores vs. permeability, (C) porosity of large pores vs. movable fluid saturation, (D) porosity of the medium pores vs. total porosity, (E) porosity of medium pores vs. permeability, (F) porosity of medium pores vs. movable fluid saturation, (G) porosity of small pores vs. total porosity, (H) porosity of small pores vs. permeability, (I) Porosity of small pores vs. movable fluid saturation, (J) porosity of micropores vs. total porosity, (K) porosity of micropores vs. permeability, and (L) porosity of micropores vs. movable fluid saturation.

Throat systems likewise correlate positively with reservoir quality parameters, although large and small throats again display weak relationships (R2 = 0.0612–0.3402; Figures 15A–C, G–I). Medium throats correlate most strongly with total porosity and permeability (R2 = 0.7499 and 0.6584, respectively; Figures 15D,E), but less so with movable fluid saturation (R2 = 0.3939; Figure 15F).

FIGURE 15

Nine scatter plots labeled A to I, each showing relationships between porosity and permeability or movable fluid saturation, differentiated by throat size: large (orange), medium (green), and small (blue). Each plot includes a trend line, equation, and R-squared value indicating the correlation.

Effect of the throat system on reservoir quality. (A) Porosity of large throats vs. total porosity, (B) porosity of large throats vs. permeability, (C) porosity of large throats vs. movable fluid saturation, (D) porosity of medium throats vs. total porosity, (E) porosity of medium throats vs. permeability, (F) porosity of medium throats vs. movable fluid saturation, (G) porosity of small throat vs. total porosity, (H) porosity of small throats vs. permeability, and (I) porosity of small throats vs. movable fluid saturation.

These results indicate that both total porosity and permeability are predominantly controlled by medium pores dominated by residual intergranular pores and medium throats composed of tubular/sheet throats. The abundance of these pores and throats is inversely proportional to compaction intensity. Thus, under relatively weak compaction, primary pores are better preserved and larger tubular throats develop more readily. Small pores, formed by intragranular dissolution, play a secondary role, with their development scaling with dissolution intensity. Medium pores also serve as the principal storage space for movable fluids, owing to their combination of a relatively large pore size and the highest porosity fraction.

For the target strata, relatively weak compaction emerges as the key factor in forming high-quality tight sandstone reservoirs, while dissolution processes provide an additional enhancement to reservoir performance. Future exploration should therefore emphasize reconstructing regional burial histories and clarifying the mechanisms of dissolution development.

5 Conclusion

This study integrates HPMI, CRMI, and NMR to characterize full-scale pore and throat distributions in tight sandstones, computes fractal dimensions using appropriate models, classifies pore–throat systems by fractal characters, identifies their genetic types, and evaluates each type’s impact on reservoir quality. The main conclusions are

  • Fractal behavior varies across scales. Seven genetic pore–throat systems are recognized: small bundle-like throats developed within clay interstitial filler, medium tubular/sheet throats generated by intense compaction, large throats formed by local dilation of tubular/sheet throats, micropores created by localized constriction of submicron-micron sized intergranular pores, small pores dominated by intergranular dissolution pores, medium pores comprised mainly of residual intergranular pores, and large pores resulting from the combination of moldic pores and residual intergranular pores.

  • 2.

    Small and medium throats conform to the capillary tube assumption, with DT1 = 2.1168–2.3923 (mean 2.2093) and DT2 = 2.4098–2.9393 (mean 2.7214). Small, medium, and large pores follow the spherical pore assumption, yielding DP2 = 2.4182–2.9902 (mean 2.8180), DP3 = 2.3177–2.9661 (mean 2.7435), and DP4 = 2.8701–2.9988 (mean 2.9825), respectively. Large throats and micropores overlap in size and form beaded features; under standard models, their computed fractal dimensions fall outside the ideal 2–3 range. Consequently, tight sandstone storage is best conceptualized as a ternary network of capillary-like throats, bead-like pore throats, and spherical pores.

  • 3.

    Correlation analysis shows that total porosity and permeability are governed primarily by medium pores and medium throats, with small pores as a secondary influence. Medium pores also provide the main space for movable fluids. Relatively weak compaction emerges as the key factor for high-quality reservoir development in the strata studied, while dissolution further enhances reservoir quality to a lesser degree.

Statements

Data availability statement

The raw data supporting the conclusions of this article will be made available by the authors, without undue reservation.

Author contributions

LF: Conceptualization, Methodology, Writing – original draft, Formal analysis, Investigation. RW: Data curation, Project administration, Resources, Writing – review and editing. NL: Software, Validation, Writing – review and editing. ZG: Supervision, Visualization, Writing – review and editing.

Funding

The authors declare that no financial support was received for the research and/or publication of this article.

Conflict of interest

Authors LF, RW, NL, and ZG were employed by the Natural Gas Research Institute of Yanchang Petroleum (Group) Co., Ltd.

Generative AI statement

The authors declare that no Generative AI was used in the creation of this manuscript.

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Summary

Keywords

controlling factor, ternary pore–throat structure, pore–throat system, fractal dimension, full-scale, reservoir, tight sandstone

Citation

Feng L, Wang R, Liu N and Gao Z (2026) Fractal characteristics of full-scale pores and throats in tight sandstone and their application in the analysis of the main controlling factors of a reservoir. Front. Earth Sci. 13:1701181. doi: 10.3389/feart.2025.1701181

Received

08 September 2025

Revised

11 November 2025

Accepted

26 November 2025

Published

06 January 2026

Volume

13 - 2025

Edited by

Li Ang, Jilin University, China

Reviewed by

Hongjian Zhu, Yanshan University, China

Jinsui Wu, Khalifa University, United Arab Emirates

Updates

Copyright

*Correspondence: Linjie Feng,

Disclaimer

All claims expressed in this article are solely those of the authors and do not necessarily represent those of their affiliated organizations, or those of the publisher, the editors and the reviewers. Any product that may be evaluated in this article or claim that may be made by its manufacturer is not guaranteed or endorsed by the publisher.

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