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ORIGINAL RESEARCH article

Front. Nutr.

Sec. Nutrition and Food Science Technology

This article is part of the Research TopicRheological Properties of Functional and Future FoodsView all 6 articles

Valorization of Canary Seeds Lipid Fraction and Defatted Flour by Supercritical Carbon Dioxide Extraction

Provisionally accepted
Esther  TriguerosEsther Trigueros1Marina  VillanuevaMarina Villanueva2M. Teresa  SanzM. Teresa Sanz1Alba  Esther IlleraAlba Esther Illera1FELICIDAD  RONDAFELICIDAD RONDA2*
  • 1Universidad de Burgos, Burgos, Spain
  • 2University of Valladolid, Valladolid, Spain

The final, formatted version of the article will be published soon.

Canary seeds (Phalaris canariensis L.) are rich in starch, proteins, and lipids, especially polyunsaturated fatty acids, however their potential remains underexplored. This study evaluated supercritical CO2 extraction (SCCO2) to obtain valuable lipids and defatted flour, evaluating the chemical characterization of the extracted oils and a thorough assessment of the properties of the resulting defatted flours. Refined (RF) and whole (WF) flours were defatted by SCCO2 (41±1 ºC, 40±1 MPa, 360-540 min) and compared with hexane extraction (HX) (80 ºC). The fatty acid profile of the lipid fraction of RF and WF revealed no significant differences, both being rich in mono- (14g/100g-oil) and polyunsaturated (76g/100g-oil) fatty acids. Unlike HX, SCCO2 preserved the tocopherol content in the extracted oil, with γ-tocopherol being the most abundant form. WF exhibited better hydration and surfactant properties than RF after defatting. Defatted flours showed increased peak (19-38%) and breakdown (20-45%) viscosities respect to the original flours due to lipids limiting water absorption. SCCO2-defatted flours showed the highest amylose retrogradation, with setback viscosity up to 26% higher than non-defatted samples. All flours studied showed the ability of forming gels with a predominantly elastic character. Gels made with SCCO2-extracted flours showed an increased elastic modulus (+20%) with respect to HX-extracted ones indicating an increased elastic behavior. In conclusion, SCCO2-extracted oil contained valuable polyunsaturated fatty acids and preserved tocopherols, whereas defatted flours improved functional and gelling properties, making them promising food thickening agents.

Keywords: Canaryseed, Functional Food, Gel rheological properties, gluten-free, PUFAs, Supercritical CO2, Tocopherols

Received: 18 Dec 2025; Accepted: 05 Feb 2026.

Copyright: © 2026 Trigueros, Villanueva, Sanz, Illera and RONDA. This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) or licensor are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms.

* Correspondence: FELICIDAD RONDA

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